Method for jointly extracting hesperidin and pectin from citrus peels
A technology of citrus peel and hesperidin, which is applied in the deep processing field of comprehensive utilization of citrus peel, can solve the problems of inability to guarantee the color of low-molecular-weight pectin, inability to meet market demand, decolorization of pectin extract, etc., and maintain normal osmotic pressure of blood vessels. , the production conditions are easy to implement, and the effect of reducing production costs
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Embodiment 1
[0030] A method for jointly extracting hesperidin and pectin from orange peel, the specific steps are as follows.
[0031] (1) Raw material pretreatment
[0032] Made from dried citrus peels. Dried citrus peels were pulverized into powders with a particle size of 0.5 mm with a pulverizer to obtain citrus peel powders.
[0033] (2) Preparation of hesperidin product
[0034] ①Extraction of hesperidin
[0035] After the first step (1) is completed, first according to the mass (g) of the citrus peel powder obtained in the step (1): the ratio of the volume (mL) of water is a ratio of 1: 10, and the described citrus peel powder is added to the into water, stir and disperse into a mixed solution, adjust the pH value of the mixed solution to 4 with hydrochloric acid for the first time, and stir for 120 minutes; adjust the pH value of the mixed solution to 10 with powdered calcium oxide for the second time, and stir for 20 minutes, so that The citrus peel powder is hardened, which ...
Embodiment 2
[0048] A method for jointly extracting hesperidin and pectin from citrus peel, same as embodiment 1, wherein:
[0049] In step (1), pulverize to a powder with a particle size of 0.1 mm.
[0050] In the 2nd (2)-1. step, the mass (g) of citrus peel powder: the ratio of the volume (mL) of water is 1: 5, and the pH value of adjusting mixed solution with hydrochloric acid is 3 for the first time, and stirring time is 30min; For the second time, use powdered calcium oxide to adjust the pH value of the mixed solution to 9, and the stirring time is 10 minutes; for the third time, use sodium hydroxide solution to adjust the pH value of the mixed solution to 12, heat to 40°C and keep it warm, and the rotation speed is 60r / min , the extraction time is 30min. The mass (g) of filter cake: the ratio of the volume (mL) of water is 1: 3, the pH value of mixed solution is adjusted to 12 with sodium hydroxide solution, is heated to 40 ℃ and is incubated, and rotating speed is 60r / min, extracti...
Embodiment 3
[0057] A method for jointly extracting hesperidin and pectin from citrus peel, same as embodiment 1, wherein:
[0058] In the step (1), the raw material is fresh orange peel. Use a shredder to chop to a powder with a particle size of 2 mm.
[0059]In the 2nd (2)-1. step, the mass (g) of citrus peel powder: the ratio of the volume (mL) of water is 1: 20, and the pH value of adjusting mixed solution with sulfuric acid is 5 for the first time, and stirring time is 240min; For the second time, the pH value of the mixed solution was adjusted to 11 with powdered calcium hydroxide, and the stirring time was 40 minutes; min, the extraction time is 120min. The mass (g) of filter cake: the ratio of the volume (mL) of water is 1: 10, the pH value of mixed solution is adjusted to 13 with potassium hydroxide solution, is heated to 70 ℃ and is incubated, and rotating speed is 120r / min, extraction time 120min.
[0060] In step (2)-②, the pH of the hesperidin extract was adjusted to 5 wit...
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