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Method for preparing biodiesel by using cinnamomum burmannii tree seed oil

A technology of biodiesel and yin xiang, which is applied in the direction of biofuel, fat oil/fat production, fat oil/fat refining, etc., can solve the problems of restricting the development of oil crops, rising edible oil imports, and unable to meet the demand for edible oil, etc.

Inactive Publication Date: 2014-09-03
JIANGXI AGRICULTURAL UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

my country is currently still in the stage of vegetable oil shortage. Although the annual output of oil crops exceeds 10 million tons, it still cannot meet the demand for edible oil, and the import of edible oil is still increasing year by year. At the same time, the shortage of cultivated land in our country has further restricted development of oil crops

Method used

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  • Method for preparing biodiesel by using cinnamomum burmannii tree seed oil
  • Method for preparing biodiesel by using cinnamomum burmannii tree seed oil

Examples

Experimental program
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Effect test

Embodiment 1

[0021] 1. Cinnamomum yin tree seed treatment

[0022] Wash the seeds of Cinnamomum sinensis, dry them in an oven at 50°C for 2.0 h, remove the water, take an appropriate amount, put them in a pulverizer, and sieve them with a 40-mesh sieve and put them in a desiccator for later use.

[0023] 2. Ultrasonic extraction of yin xiang oil

[0024] Take an appropriate amount of Cinnamomum sinensis seed powder and put it in a triangular flask, add petroleum ether according to the ratio of material to liquid 1:10, extract at 60 °C, and extract for 20 min at an ultrasonic power of 105 W, and filter to obtain a light yellow filtrate, which is transferred to a round bottom flask middle. Atmospheric distillation first, and then vacuum distillation to remove petroleum ether. The obtained Cinnamomum burmanii seed oil was dried in an oven at 100°C±5°C for 30 min to obtain bright yellow Cinnamomum burmanii seed oil.

[0025] 3. Deacidification pretreatment of yin xiang tree seed oil

[0...

Embodiment 2

[0035] 1. Cinnamomum yin tree seed treatment

[0036] Wash the seeds of Cinnamomum sinensis, dry them in an oven at 50°C for 2.0 h, remove the water, take an appropriate amount, put them in a pulverizer, and sieve them with a 40-mesh sieve and put them in a desiccator for later use.

[0037] 2. Ultrasonic extraction of yin xiang oil

[0038]Take an appropriate amount of Cinnamomum sinensis seed powder and put it in a conical flask, add petroleum ether at a material-to-liquid ratio of 1:10, extract at a temperature of 60°C, and extract at an ultrasonic power of 105W for 20 minutes. Suction filter to obtain a light yellow filtrate, which is then transferred to a round-bottomed flask. Atmospheric distillation first, and then vacuum distillation to remove petroleum ether. Put the obtained yamba seed oil into an oven and dry at 100°C±5°C for 30 minutes to obtain bright yellow yamba seed oil.

[0039] 3. Deacidification pretreatment of yin xiang tree seed oil

[0040] Take ...

Embodiment 3

[0049] 1. Cinnamomum yin tree seed treatment

[0050] Wash the seeds of Cinnamomum sinensis, dry them in an oven at 50°C for 2.0 h, remove the water, take an appropriate amount, put them in a pulverizer, and sieve them with a 40-mesh sieve and put them in a desiccator for later use.

[0051] 2. Ultrasonic extraction of yin xiang oil

[0052] Take an appropriate amount of Cinnamomum sinensis seed powder and put it in a conical flask, add petroleum ether at a material-to-liquid ratio of 1:10, extract at a temperature of 60°C, and extract at an ultrasonic power of 105W for 20 minutes. Suction filter to obtain a light yellow filtrate, which is then transferred to a round-bottomed flask. Atmospheric distillation first, and then vacuum distillation to remove petroleum ether. Put the obtained yamba seed oil into an oven and dry at 100°C±5°C for 30 minutes to obtain bright yellow yamba seed oil.

[0053] 3. Deacidification pretreatment of yin xiang tree seed oil

[0054] Take an ap...

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Abstract

The invention mainly discloses a method for preparing biodiesel by using cinnamomum burmannii tree seed oil. The method is characterized in that wild woody oil plant cinnamomum burmannii tree seed oil is taken as the raw material, and the biodiesel is prepared by catalytic ester exchange reaction after methanol extraction deacidification. Various indexes of the cinnamomum burmannii oil biodiesel are close to main performance indexes of national GB / T20828-2007 Biodiesel for Blending Diesel Fuel of 0# diesel oil in China, and moreover, and the cinnamomum burmannii oil biodiesel is high in flash point and good in safety, high in cetane number (CN) and good in combustibility. The cinnamomum burmannii tree seed oil is wild woody tallow species, and excellent tree species are obtained after directive breeding and reproducing; cost of biodiesel raw material can be greatly lowered after planting the tree species in a large area; moreover, the cinnamomum burmannii tree is very strong in stress resistance, can effectively utilize barren mountains, barren land, desert, and the like, and has significance in improving and protecting ecological environment of China.

Description

technical field [0001] The invention relates to a method for preparing biodiesel from seed oil of a wild woody oil plant, Cinnamomum annua. technical background [0002] The 21st century will face severe challenges of energy issues, and the development and utilization of renewable energy is a major issue related to the sustainable development of China's national economy, national security and social progress. Biodiesel is a fatty acid monoester produced by esterification of vegetable oil or animal fat. Due to its renewability and excellent environmental performance, it has become an ideal fuel to replace fossil fuel oil. At present, various oil crops such as rapeseed oil, soybean oil, and cottonseed oil have been widely used as raw materials for biodiesel production in European and American countries. my country is currently still in the stage of vegetable oil shortage. Although the annual output of oil crops exceeds 10 million tons, it still cannot meet the demand for edib...

Claims

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Application Information

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IPC IPC(8): C11C3/10C11B1/10C11B1/00C11B3/02C11B3/12C11B3/00C10L1/02
CPCY02E50/13Y02E50/10
Inventor 刘光斌董振浩赵晓霞
Owner JIANGXI AGRICULTURAL UNIVERSITY