Fabric coating slurry and preparing method thereof

A technology for coating pulp and fabrics, which is applied in textiles, papermaking, and fiber treatment, etc. It can solve the problems of poor oil resistance and water resistance, poor light stability and thermal stability, and small contact angle of the film to achieve oil resistance. And the effect of excellent water resistance, good fullness and good weather resistance

Active Publication Date: 2014-11-12
甄曰菊
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] However, the light stability and thermal stability of the current fabric coating slurry are poor, especially the polyurethane solid content used is very low, the particle size is large and uneven,

Method used

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  • Fabric coating slurry and preparing method thereof
  • Fabric coating slurry and preparing method thereof
  • Fabric coating slurry and preparing method thereof

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0029] Example 1

[0030] It adopts the following method to prepare epoxy soybean oil modified waterborne polyurethane:

[0031] First, add epoxidized soybean oil, diethanolamine and isopropanol to the reactor, heat up to 75°C, add tetrafluoroboric acid catalyst, keep the temperature for 20 hours, after the reaction, distill out isopropanol, wash with water and dry to obtain the ring Oxygen soybean oil polyol, wherein the mass of diethanolamine is 70% of the mass of epoxy soybean oil; the isopropanol is 200% of the mass of epoxy soybean oil; the tetrafluoroboric acid is 5% of the mass of epoxy soybean oil ;

[0032] Then, under the protection of nitrogen, the obtained epoxidized soybean oil polyol, polyoxypropylene glycol, and dicyclohexylmethane diisocyanate are added to the reactor, and the polyoxypropylene glycol is of epoxy soybean oil polyol quality 10%, the dicyclohexylmethane diisocyanate is 5% of the mass of the epoxy soybean oil polyol; the temperature is raised to 85°C, t...

Example Embodiment

[0035] Example 2

[0036] It adopts the following method to prepare epoxy soybean oil modified waterborne polyurethane:

[0037] First, add epoxidized soybean oil, diethanolamine and isopropanol to the reactor, heat to 77°C, add tetrafluoroboric acid catalyst, keep it for 24 hours, after the reaction is over, distill out isopropanol, wash with water and dry to obtain ring Oxygen soybean oil polyol, wherein the mass of diethanolamine is 85% of the mass of epoxy soybean oil; the isopropanol is 225% of the mass of epoxy soybean oil; the tetrafluoroboric acid is 5% of the mass of epoxy soybean oil ;

[0038] Then, under the protection of nitrogen, the obtained epoxidized soybean oil polyol, polyoxypropylene glycol, and dicyclohexylmethane diisocyanate are added to the reactor, and the polyoxypropylene glycol is of epoxy soybean oil polyol quality 13%, the dicyclohexylmethane diisocyanate is 6% of the mass of the epoxy soybean oil polyol; the temperature is raised to 87°C, and the organ...

Example Embodiment

[0041] Example 3

[0042] It adopts the following method to prepare epoxy soybean oil modified waterborne polyurethane:

[0043] First, add epoxidized soybean oil, diethanolamine and isopropanol to the reactor, heat up to 80°C, add tetrafluoroboric acid catalyst, keep it for 28 hours, after the reaction, distill out isopropanol, wash with water and dry to obtain the ring Oxygen soybean oil polyol, wherein the mass of diethanolamine is 100% of the mass of epoxy soybean oil; the isopropanol is 250% of the mass of epoxy soybean oil; and the tetrafluoroboric acid is 5% of the mass of epoxy soybean oil ;

[0044] Then, under the protection of nitrogen, the obtained epoxidized soybean oil polyol, polyoxypropylene glycol, and dicyclohexylmethane diisocyanate are added to the reactor, and the polyoxypropylene glycol is of epoxy soybean oil polyol quality 15%, the dicyclohexylmethane diisocyanate is 7% of the mass of the epoxy soybean oil polyol; the temperature is raised to 90°C, and the o...

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Abstract

The invention discloses fabric coating slurry which is prepared by the following components, by weight, of 100 parts of epoxidized soybean oil modified waterborne polyurethane, 5-10 parts of crosslink type macromolecule emulsion thickening agents BJ-100 and 5-10 parts of fabric coating extrusion dispersing agents PTFE D-210. The invention discloses a preparing method of the fabric coating slurry at the same time. The fabric coating slurry is well improved in light stability, heat stability, oil resistance and water resistance.

Description

technical field [0001] The invention relates to an environment-friendly fabric coating slurry, in particular to a fabric coating slurry prepared by using epoxy soybean oil modified water-based polyurethane, and to a preparation method of the fabric coating slurry. Background technique [0002] At present, in the textile industry, polyurethane has shown good performance in printing and dyeing auxiliaries and finishing agents. Fabric coating finishing is to coat a thin film on the surface of textiles, so that the fabrics have certain special functions (such as anti-wrinkle, light-shielding, water-repellent, oil-proof, flame-retardant, warm, imitation down, reflective, breathable, etc.) ) or appearance style. Because water-based polyurethane does not contain organic solvents such as formaldehyde, it has become the development direction of fabric dyeing and finishing as a formaldehyde-free fabric finishing agent. As a leather finishing agent and fabric coating glue, water-base...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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IPC IPC(8): D06M15/568D06M15/263D06M15/256C08G18/66C08G18/32C08G18/22C08G18/12
Inventor 甄曰菊
Owner 甄曰菊
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