A kind of concrete silt inhibitor based on clay mineral flocculation and preparation method thereof
A flocculation, clay mineral technology, applied in the field of concrete mud inhibitor and its preparation, can solve the problem of increasing concrete compactness, environmental pollution of sewage and sediment, concrete strength, drying shrinkage performance, impermeability, frost resistance and resistance problems such as the adverse effect of wear performance, to achieve the effect of reducing operating costs, wide application prospects and theoretical value
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Embodiment 1
[0036] 100 parts by weight of ferrous sulfate heptahydrate from industrial production are added to the synthesis container, 20 parts of water are added, the temperature is raised to 50° C., slowly dripping sulfuric acid and 10% nitric acid that account for 35% of the amount of ferrous sulfate heptahydrate, The dropping time is 0.5h, and the temperature during the whole dropping process is controlled not to exceed 60°C; after the sulfuric acid and nitric acid mixture is added dropwise, and the temperature is stabilized to 55°C, add 4.2 parts by weight of potassium permanganate and 10 parts by weight of sulfuric acid The speed of adding aluminum and potassium permanganate is based on controlling the reaction temperature without obvious rise. Potassium permanganate can be dissolved in 20 parts by weight of water and added dropwise within 45 minutes; potassium permanganate can also be insoluble in water and directly spaced Due to the large instantaneous concentration of the input a...
Embodiment 2
[0038] 100 parts by weight of ferrous sulfate heptahydrate from industrial production are added to the synthetic container, without adding water, the temperature is raised to 60° C., and slowly add sulfuric acid and 5% silicic acid that account for 25% of the amount of ferrous sulfate heptahydrate dropwise. The adding time is 45 minutes, and the temperature during the whole dropping process is controlled not to exceed 60 degrees; after the sulfuric acid and silicic acid mixture is added dropwise, and the temperature is stabilized to 60°C, 5 parts by weight of hydrogen peroxide and 15 parts by weight of zinc oxide are added. The speed of addition is subject to controlling the reaction temperature without obvious rise. Dissolve the hydrogen peroxide in 200 parts by weight of water and add it dropwise within 3 hours; the zinc oxide is directly added, and the addition time is subject to the temperature of the reactants in the container not being significantly lowered; hydrogen perox...
Embodiment 3
[0040] 100 parts by weight of ferrous sulfate heptahydrate from industrial production are added to the synthesis container, 100 parts by weight of water are added, the temperature is raised to 50° C., and the sulfuric acid that accounts for 40% of the amount of ferrous sulfate heptahydrate is slowly added dropwise, and the dropping time is 1h, the temperature of the whole dropping process is controlled not to exceed 60°C; after the sulfuric acid is added dropwise, after the temperature is stabilized to 40°C, add 10 parts by weight of aluminum sulfate, add directly, and use the pump to feed in the air for 20 hours After 20 hours, measure the concentration (solid content) of the flocculant, and then add magnesium fluorosilicate according to the compound ratio of flocculant (solid content): stabilizer: corrosion inhibitor: enhancer = 70:10:5:15 mass percent , hexamethylenetetramine, sodium nitrite, mix and stir well.
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