A kind of oil-based waterproof coating with added calcium sulfate whiskers and preparation method thereof
A calcium sulfate whisker, waterproof coating technology, applied in anti-corrosion coatings, epoxy resin coatings, coatings, etc., can solve the problems of poor water solubility and aging resistance, affecting material properties, poor thermal stability, etc., and achieve strong adhesion. , Excellent corrosion resistance and excellent performance
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Embodiment 1
[0025] Embodiment 1: a kind of oily waterproof coating that adds calcium sulfate whisker, it is made up of the raw material of following weight portion:
[0026]
[0027] The above-mentioned preparation method of adding the oily waterproof paint of calcium sulfate whisker, it may further comprise the steps:
[0028] S1. Weighing: Weigh each raw material according to the above ratio, the average length-to-diameter ratio of calcium sulfate whiskers is 50-80, and the diameter is 1-4 μm, and set aside;
[0029] S2. Modification: an aqueous ethanol solution prepared with anhydrous ethanol and deionized water at a volume ratio of 3:1, adding aluminate coupling agent, aluminate coupling agent and calcium sulfate crystals to the ethanol solution The weight ratio of the whiskers is 1:20, stir at 800r / min, add calcium sulfate whiskers, adjust the pH of the solution system to 4 with glacial acetic acid, stir at 2300r / min for 1 hour, and then vacuum dry to obtain modified sulfuric acid...
Embodiment 2
[0031] Embodiment 2: a kind of oily waterproof coating that adds calcium sulfate whisker, it is made up of the raw material of following weight portion:
[0032]
[0033]
[0034] The above-mentioned preparation method of adding the oily waterproof paint of calcium sulfate whisker, it may further comprise the steps:
[0035] S1. Weighing: Weigh each raw material according to the above ratio, the average length-to-diameter ratio of calcium sulfate whiskers is 50-80, and the diameter is 1-4 μm, and set aside;
[0036] S2. Modification: an aqueous ethanol solution prepared with anhydrous ethanol and deionized water at a volume ratio of 3:1, adding aluminate coupling agent, aluminate coupling agent and calcium sulfate crystals to the ethanol solution The weight ratio of the whiskers is 1:30, stir at 1000r / min, add calcium sulfate whiskers, adjust the pH value of the solution system to 5 with glacial acetic acid, stir at 2700r / min for 1 hour, and then vacuum dry to obtain mod...
Embodiment 3
[0038] Embodiment 3: a kind of oily waterproof coating that adds calcium sulfate whisker, it is made up of the raw material of following weight portion:
[0039]
[0040] The above-mentioned preparation method of adding the oily waterproof paint of calcium sulfate whisker, it may further comprise the steps:
[0041] S1. Weighing: Weigh each raw material according to the above ratio, the average length-to-diameter ratio of calcium sulfate whiskers is 50-80, and the diameter is 1-4 μm, and set aside;
[0042] S2. Modification: an aqueous ethanol solution prepared with anhydrous ethanol and deionized water at a volume ratio of 3:1, adding aluminate coupling agent, aluminate coupling agent and calcium sulfate crystals to the ethanol solution The weight ratio of the whiskers is 1:22, stir at a speed of 900r / min, add calcium sulfate whiskers, adjust the pH of the solution system to 4.5 with glacial acetic acid, stir at a speed of 2500r / min for 1 hour, and then vacuum dry to obtai...
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