A kind of tin dioxide electrode ceramic material and preparation method thereof
A technology of tin dioxide and ceramic materials, applied in the field of semiconductor ceramics, can solve the problems of increasing drying equipment, increasing the drying process, prolonging the production cycle, etc., achieving the effects of less production equipment, increasing volume density, and enhancing corrosion resistance
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Embodiment 1
[0027] Weigh according to the following raw material ratios: 100 kg tin dioxide powder (purity 99%), 0.2 kg copper oxide (purity 99%), 0.4 kg zinc oxide (purity 99%) 1.1 kg trioxide Antimony (purity 99%), 0.8㎏ bismuth subcarbonate, 3㎏ Baume 52% sodium silicate aqueous solution; after dry mixing additive powder and tin dioxide powder in a weight ratio of 1:5 , And then put all the remaining tin dioxide powder into the V-shaped mixer for mixing, and then add the prepared sodium silicate aqueous solution with a Baume degree of 52% to the V-shaped mixer for 5 hours, and then use Airflow screen, 600 mesh screen is sieved continuously for three times, after sieving, it is put into a rubber mold with a steel mold, and cold isostatically pressed, 160MPa-200MPa pressure is maintained for 3-5 minutes, and a green body is pressed. Body trimming: repair and smooth the surface of the body;
[0028] Drying: low-humidity drying, the temperature is controlled between 120℃-200℃ for more than 24 ...
Embodiment 2
[0031] Weigh according to the following raw material ratios: 100 kg tin dioxide powder (purity 99%), 0.3 kg copper oxide (purity 99%), 0.5 kg zinc oxide (purity 99%) 1.2 kg trioxide Antimony (purity 99%), 1.3㎏ bismuth subcarbonate, 3.5㎏ Baume of 52% sodium silicate aqueous solution; after dry mixing the additive powder and tin dioxide powder in a weight ratio of 1:5 , And then put all the remaining tin dioxide powder into the V-shaped mixer for mixing, and then add the prepared sodium silicate aqueous solution with a Baume degree of 52% to the V-shaped mixer for 5 hours, and then use Airflow screen, 600 mesh screen is sieved continuously for three times, after sieving, it is put into a rubber mold with a steel mold, and cold isostatically pressed, 160MPa-200MPa pressure is maintained for 3-5 minutes, and a green body is pressed. Body trimming: repair and smooth the surface of the body;
[0032] Drying: low-humidity drying, the temperature is controlled between 120℃-200℃ for more...
Embodiment 3
[0035] Weigh according to the following raw material ratios: 100kg tin dioxide powder (purity 99%) as main ingredient, 0.5kg copper oxide (purity 99%) as additive, 0.8kg zinc oxide (purity 99%) and 1.4kg trioxide Antimony (purity 99%), 1.5㎏ bismuth subcarbonate, 5㎏ Baume 52% sodium silicate aqueous solution; after dry mixing the additive powder and tin dioxide powder in a weight ratio of 1:5 , And then put all the remaining tin dioxide powder into the V-shaped mixer for mixing, and then add the prepared sodium silicate aqueous solution with a Baume degree of 52% to the V-shaped mixer for 5 hours, and then use Airflow screen, 600 mesh screen is sieved continuously for three times, after sieving, it is put into a rubber mold with a steel mold, and cold isostatically pressed, 160MPa-200MPa pressure is maintained for 3-5 minutes, and a green body is pressed. Body trimming: repair and smooth the surface of the body;
[0036] Drying: low-humidity drying, the temperature is controlled ...
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