Process method for producing lubricating oil base oil through poor-quality raw material
A technology for lubricating base oils and low-quality feedstock oils, applied in the petroleum industry, lubricating compositions, hydrotreating processes, etc., can solve the problems of light fraction dewaxing, mass loss, yield loss, etc. Effect of reducing hydrogen sulfide and ammonia content and increasing hydrogen partial pressure
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Embodiment 1
[0051] use figure 1 In the process flow shown, the hydrocracking in the third stage is a one-pass process, and all the hydrocracking tail oil undergoes isomerization dewaxing reaction. Hydrofinishing catalyst A is loaded in the first section, and hydrofinishing catalyst B is filled in the second section. The upper part of the refining reaction zone of the second stage adopts gas-liquid parallel flow reaction, and the lower part adopts gas-liquid countercurrent reaction, and the catalyst loading volume ratio of the parallel flow section and the countercurrent section is 1:1.
[0052] In the hydrocracking tail oil pre-fractionation tower, the tail oil is cut into three tail oil fractions. The cutting temperatures of light tail oil, intermediate tail oil and heavy tail oil are respectively 400°C and 450°C. Isomerization dewaxing reaction.
Embodiment 2
[0054] Both the first section and the second section are filled with hydrotreating catalyst B, and the others are the same as in Example 1.
Embodiment 3
[0070] The basic process of the process is as figure 1 As shown, the >370°C distillate part is recycled to the inlet of the second-stage hydrotreating reactor, and the circulation amount is 25% of the tail oil. Control the denitrification rate of the first stage reaction zone to 75wt%. The cutting temperature of the hydrocracking tail oil is the same as in Example 1.
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