Bioflavonoid coated materials
A technology of bioflavonoids and polymer materials, applied in the field of polymer materials, can solve the problems such as the application of bioflavonoid compositions that are not disclosed
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Embodiment 1
[0106] experimental method
[0107] Preparation of Citrox precursor: Citrox HXT powder was dissolved in methanol. The precursors were formulated using either 10% or 15% by weight Citrox in methanol.
[0108] Pretreatment of samples: preliminary He / O with and without polyethylene terephthalate (PET) films and silicon wafers 2 Plasma pretreatment.
[0109] In atmospheric plasma jet processing systems (such as PlasmaStream TM ) by two rounds using 5% O in He 2 The formed plasma activates the substrate. The applied plasma powder was 80%, the CNC speed was 7 mm / s, and the distance from the substrate to the plasma injection hole was 10 mm.
[0110] In reel-to-reel atmospheric plasmas (e.g. Labline TM system) by making the substrate formed between two insulating plates containing 5% O in He 2 The processing chamber passes through three times to activate the substrate. The plasma powder was applied at 1000 W and the sample was passed through the chamber at a velocity of 1.5 m / ...
Embodiment 2
[0155] Impregnation of polystyrene sheets with Citrox
[0156] Polystyrene sheets were treated using plasma immersion ion implantation (PIII) with nitrogen ions at an energy of 20 keV for 800 seconds to form a surface embedded with groups capable of covalently binding bioactive molecules (as in Bilek et al., PNAS, 08( 35):14405-14410, 2011, which is hereby incorporated by reference). PIII-treated and untreated sheets were incubated for 3 hours in tubes filled with Citrox concentrate (PHLC 45) or deionized water (for controls). Contains bioflavonoids in HPLC 45 or "Citrox BC" 45% (total composition of HPLC 45 / Citrox BC). The bioflavonoids were in admixture with biomass residues extracted from bitter oranges such as pectin, sugars and small amounts of organic acids (which constituted the remaining 55%). HPLC 45 is available from Exquim (a company of Grupo Ferrer) as Citrus Bioflavonoid Complex 45% HPLC. After incubation, the sheets were washed thoroughly in the tubes with dei...
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