Novel preparation method for natural taurine
A technology of taurine and a new method, applied in the direction of chemical instruments and methods, preparation of organic compounds, organic chemistry, etc., can solve the problems of difficult industrial production, increased production investment, and large ethanol consumption, so as to avoid the source of raw materials The effect of restriction, low ethanol consumption, and high extraction rate
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Embodiment 1
[0034] Embodiment 1: the extraction of natural taurine
[0035] (1) Source of raw materials: collect 1 L of cooking broth produced in the process of processing variegated clams, oysters, meretrix meretrix, mussels, and scallops in the factory, totaling 5 L, and mix well to obtain the extract;
[0036] (2) Concentration for the first time: Concentrate the extract to 1 L;
[0037] (3) Alcohol precipitation: Add 3 L of 95% ethanol by volume to 1 L of the concentrated extract to obtain the precipitate and supernatant, and extract 2.6 L of the supernatant;
[0038] (4) Second concentration: Concentrate 2.6 L of the supernatant to 105 mL, with a soluble solid content of 45.7%, and adjust its pH to 5.16, which is the concentrated solution;
[0039] (5) Crystallization: put 105 mL of the concentrated solution with a pH of 5.16 in a low-temperature environment of -30 °C, add a little taurine seed crystals, and stir slowly for more than 12 h, the taurine crystals are precipitated, and...
Embodiment 2
[0041] Embodiment 2: the extraction of natural taurine
[0042] (1) Source of raw materials: collect 1 kg of discarded internal organs produced during the processing of octopus, squid, and cuttlefish in the factory, totaling 3 kg;
[0043] (2) Water extraction: Add 15 L of water to 3 kg of discarded viscera, cook at 120°C for 60 min, and filter to obtain 14.8 L of extract;
[0044] (3) Concentration for the first time: Concentrate 14.8 L of extract to 1.5 L;
[0045] (4) Alcohol precipitation: Add 2 L of 95% ethanol by volume to the concentrated 1.5 L extract to obtain the precipitate and supernatant, and extract 2.1 L of the supernatant;
[0046] (5) Second concentration: Concentrate 2.1 L of the supernatant to 70 mL with a soluble solid content of 50.1%, which is the concentrated solution;
[0047](6) Crystallization: Place 70 mL of the concentrated solution in a low-temperature environment of -15 °C, add a little taurine seed crystals, and stir slowly for more than 12 h...
Embodiment 3
[0049] Embodiment 3: the extraction of natural taurine
[0050] (1) Source of raw materials: Collect 5 kg of discarded internal organs produced in the process of processing abalone in the factory, and fully crush them with a meat grinder;
[0051] (2) Water extraction: Add 17.5 L of water to 5 kg of crushed abalone viscera, cook at 80°C for 120 min, and filter to obtain 17.2 L of extract;
[0052] (3) Concentration for the first time: Concentrate 17.2 L of extract to 2.3 L;
[0053] (4) Alcohol precipitation: Add 4.6 L of 95% ethanol by volume to the concentrated 2.3 L extract to obtain the precipitate and supernatant, and extract 5 L of the supernatant;
[0054] (5) Second concentration: Concentrate 5 L of supernatant to 200 mL, with a soluble solid content of 45.5%, and adjust its pH to 5.16, which is the concentrated solution;
[0055] (6) Crystallization: put 200 mL of the concentrated solution in a low-temperature environment of -20 °C, add a little taurine seed cryst...
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