A co 2 electrochemical reduction method
A working electrode and electrochemical technology, which is applied in the direction of electrodes, electrolytic processes, electrolytic components, etc., can solve the problems of low Faraday efficiency, low reduction current density, and small amount of reduction products, so as to prevent negative effects, suppress side reactions, The effect of improving product efficiency
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specific Embodiment approach 1
[0015] Specific implementation mode 1: This implementation mode is a CO with an Ag-containing electrode as the working electrode. 2 The electrochemical reduction method is specifically completed according to the following steps: 1. Configure the electrolyte: mix the ionic liquid and ultrapure water to obtain an electrolyte, and the molar fraction of the ionic liquid in the electrolyte is 40%; 2. Equipment assembly: The electrolytic cell of the three-electrode system is arranged in an H shape, that is, the electrolytic cell is divided into an anode pool and a cathode pool, and the anode pool and the cathode pool are connected by a channel. Separated from the anode pool, pour the electrolyte solution into the electrolytic cell of the three-electrode system until the channel between the anode pool and the cathode pool is filled with electrolyte solution, use the platinum sheet as the counter electrode, and place the counter electrode in the three-electrode system. In the anode ar...
specific Embodiment approach 2
[0017] Specific embodiment two: the difference between this embodiment and specific embodiment one is: the ionic liquid described in step one is BMIM-BF 4 、EMIM-BF 4 、EMIM-NTF 2 , EMIM-DCA, EMIM-EtSO 4 or EMIM-OAC. Others are the same as the first embodiment.
specific Embodiment approach 3
[0018] Embodiment 3: The difference between this embodiment and Embodiment 1 or 2 is that the Ag-containing electrode described in step 2 is an Ag sheet, a porous Ag sheet, an Ag sheet with an AgO oxide film on the surface, or an Ag particle electrode. Or an Ag particle electrode with an AgO film on the surface. Others are the same as those in Embodiment 1 or 2.
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