A kind of preparation method of colored electromagnetic shielding fabric
A colored electromagnetic and fabric technology, applied in the textile field, can solve the problem of single color tone of polyaniline electromagnetic shielding fabrics, achieve excellent electromagnetic shielding performance, and improve the effect of dyeing fastness
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Embodiment 1
[0016] (1) Dissolve 0.01g of basic fuchsin in 300mL of deionized water, stir well, and after it is completely dissolved, transfer it to a water bath at 40°C; then immerse 10g of fully wetted cotton fabric into the dye solution Add 6g of sodium chloride after 15 minutes, and continue dyeing for 30 minutes under stirring conditions. After dyeing, cool down, take out the fabric, and wash it with deionized water for 3 times; In the 2g / L soaping solution, after soaping at 90°C for 15 minutes, wash with deionized water for 3 times, and dry at 60°C.
[0017] (2) Immerse the above-mentioned textiles in the reaction solution of 0.5mol / L hydrochloric acid and 10g / L ammonium persulfate, continue to stir evenly, oxidatively polymerize at 0°C for 18h, after the reaction, wash 3 times with acetone and distilled water respectively, and wash at 50°C After drying, the colored electromagnetic shielding fabric is obtained.
Embodiment 2
[0022] (1) Dissolve 0.5g of methylene green in 500mL of deionized water, stir well, and after it is completely dissolved, transfer it to an 80°C water bath; then immerse 10g of fully wetted viscose fabric into the dye solution After 15 minutes, add 30 g of anhydrous sodium sulfate, and continue dyeing for 75 minutes under stirring conditions. After dyeing, cool down, take out the fabric, and wash it with deionized water for 5 times; In the soaping solution with a concentration of 3g / L, after soaping at 95°C for 10 minutes, wash with deionized water for 5 times, and dry at 80°C.
[0023] (2) Immerse the above-mentioned textiles in the reaction solution of 2mol / L p-toluenesulfonic acid and 30g / L sodium persulfate, continue to stir evenly, oxidatively polymerize at 5°C for 5 hours, after the reaction, wash with acetone and distilled water 5 times respectively, Dry at 80°C to obtain a colored electromagnetic shielding fabric.
Embodiment 3
[0027] (1) Dissolve 0.2g of acridine orange in 400mL of deionized water, stir well, and after it is completely dissolved, transfer it to a 60°C water bath; then immerse 10g of fully wetted pure hemp fabric into the dyeing solution After 15 minutes, add 16g of sodium chloride, and continue dyeing for 60 minutes under stirring conditions. After dyeing, cool down, take out the fabric, and wash it with deionized water for 4 times; In the 2.5g / L soaping solution, after soaping at 92°C for 12 minutes, wash with deionized water 4 times, and dry at 70°C.
[0028] (2) Immerse the above-mentioned textiles in the reaction solution of 1mol / L sulfuric acid and 20g / L potassium persulfate, continue to stir evenly, oxidatively polymerize at 2°C for 10h, after the reaction, wash 4 times with acetone and distilled water respectively, and dry at 60°C After drying, a colored electromagnetic shielding fabric is obtained.
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