Nanofiber multilayer combined filter mask and production method thereof
A nanofiber, multi-layer composite material technology, applied in the field of daily necessities, can solve the problems of large specific surface area, unsatisfactory, easy to suffocate, etc., and achieves the effect of good air permeability and improved filtration efficiency.
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Embodiment 1
[0030] The present invention, a preparation method of a nanofiber multi-layer composite filter mask, specifically comprises the following steps:
[0031] Step 1. Dissolve the dried nylon 6 particles in anhydrous formic acid solvent to prepare a polymer nanofiber solution with a mass fraction of 15%;
[0032] Step 2. Add the polymer nanofiber solution in step 1 into the electrospinning device, the voltage is 100,000 volts, the receiving distance is 290 mm, PP spunbond non-woven fabric is selected as the receiving substrate, and the running speed of the substrate is 450 mm / min, to obtain the monomer material of the spunbond non-woven fabric and the polymer nanofibers, wherein the diameter of the polymer nanofibers is about 60 nm;
[0033] Step 3. Compound the above-mentioned monomer materials in three layers to obtain a three-layer composite material. After testing, the filtration efficiency of this three-layer composite material can reach 90%, and the resistance is about 9mmH ...
Embodiment 2
[0035] The present invention, a preparation method of a nanofiber multi-layer composite filter mask, specifically comprises the following steps:
[0036] Step 1. Dissolve the dried nylon 6 particles in anhydrous formic acid solvent to prepare a polymer solution with a mass fraction of 15%;
[0037] Step 2. Add the polymer nanofiber solution in step 1 into the electrospinning device, the voltage is 100,000 volts, the receiving distance is 290 mm, the melt-blown non-woven fabric is selected as the receiving substrate, and the running speed of the substrate is 400 mm / min, coating one side of the melt-blown non-woven fabric to obtain the monomer material of the melt-blown non-woven fabric and the polymer nanofibers;
[0038] Step 3. The other side of the above-mentioned monomer material on one side is coated with polymer nanofibers. The method is the same as that in step 2. After coating, a composite composite with polymer nanofibers coated on both sides is obtained. Material, i...
Embodiment 3
[0040] The present invention, a preparation method of a nanofiber multi-layer composite filter mask, specifically comprises the following steps:
[0041] Step 1. Dissolve the dried nylon 6 particles in anhydrous formic acid solvent to prepare a polymer solution with a mass fraction of 15%, which is called polymer nanofiber solution 1; dissolve the weighed PVDF in N,N - In dimethylformamide (DMF) solvent, a polymer solution with a mass fraction of 18% is prepared, which is called polymer nanofiber solution II;
[0042] Step 2. First, the polymer nanofiber solution is added to the electrospinning device, the voltage is 100,000 volts, the receiving distance is 290 mm, the PP non-woven fabric is the receiving substrate, and the running speed of the substrate is 450 mm / min to obtain Monomer material 1 of nylon 6 and PP non-woven fabrics, wherein the diameter of nylon 6 nanofibers is about 60nm;
[0043]Step 3. Add the polymer nanofiber solution 2 into the electrospinning device, t...
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Abstract
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