Polymer composite for board modification and preparation method thereof
A technology of composite materials and polymers, which is applied in the field of polymer composite materials for plate modification and its preparation, can solve the problems of weak strength, thin waterproof layer, and inability to withstand erosion, etc., and achieve dense and good hardened plates. Excellent outdoor durability and convenient construction
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[0033] The preparation method of the polymer composite material for plate modification comprises the following steps: weighing each component by weight,
[0034] 1) Premix the polymer monomer and modifier with 19 / 20 of the total amount of polymer monomer to obtain a mixture of polymer monomer and modifier, which is ready for use;
[0035] 2) Put the protective colloid and water into the reactor, control the temperature at 80-90°C, and stir for 30-60min;
[0036] 3) feeding into the reactor is nitrogen or carbon dioxide with a concentration of 99%, and adding an acid solution to adjust the pH value=3-5;
[0037] 4) continue to drop the polymer monomer of 1 / 20 of the total amount of polymer monomer into the reaction kettle, and stir for 15-20min;
[0038] 5) drop into the initiator of 1 / 20 of the total amount of polymer monomers in the reactor, stir for 25-35min;
[0039] 6) dropwise adding the polymer monomer and modifier mixture obtained in step 1) and the remaining initiato...
Example Embodiment
[0043] Example 1
[0044] A preparation method of a polymer composite material for plate modification comprises the following steps:
[0045] 1) Weigh the following components by weight: 296 parts of polymer monomers, 30 parts of modifiers, 9 parts of protective colloids, 2 parts of initiators, and 450 parts of deionized water;
[0046] 2) Pre-mixing 19 / 20 of the total amount of polymer monomers with the modifier and the polymer monomer to obtain a mixture of the polymer monomer and the modifier, ready for use;
[0047] 3) Put the protective colloid and water into the reaction kettle, control the temperature at 80-90°C, and stir for 45min;
[0048] 4) pass into the nitrogen or carbon dioxide that concentration is 99% in the reactor, and add acid solution and adjust pH value=4;
[0049] 5) continue to drop the polymer monomer of 1 / 20 of the total amount of polymer monomer into the reactor, stir for 18min;
[0050] 6) drop the initiator of 1 / 20 of the total amount of polymer ...
Example Embodiment
[0055] Example 2
[0056] A preparation method of a polymer composite material for plate modification comprises the following steps:
[0057] 1) Weigh the following components by weight: 296 parts of polymer monomers, 20 parts of modifiers, 6 parts of protective colloids, 1.5 parts of initiators, and 300 parts of distilled water;
[0058]2) Pre-mixing 19 / 20 of the total amount of polymer monomers with the modifier and the polymer monomer to obtain a mixture of the polymer monomer and the modifier, ready for use;
[0059] 3) put the protective colloid and water into the reaction kettle, control the temperature at 80-90°C, and stir for 30min;
[0060] 4) pass into the nitrogen or carbon dioxide that concentration is 99% in the reactor, and add acid solution and adjust pH value=3;
[0061] 5) continue to drop the polymer monomer of 1 / 20 of the total amount of polymer monomer into the reactor, stir for 15min;
[0062] 6) drop into the initiator of 1 / 20 of the total amount of po...
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