Use of SrCuSi4O10 two-dimensional crystal and saturated absorber device formed by the same
A technology of two-dimensional crystals and absorbers, which is applied in the field of nonlinear optical materials and devices, can solve problems such as application limitations of multi-atomic layer graphene, achieve excellent saturated absorption characteristics, and reduce costs
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Embodiment 1
[0025] This example illustrates how to prepare SrCuSi supported in the polymer polyvinyl alcohol (PVA) 4 o 10 Saturable absorbers in two-dimensional crystals.
[0026] (1) 0.15g of SrCuSi 4 o 10 The crystals were added to 20ml hydrochloric acid solution of 3mol / L, ultrasonically treated, and left to stand for 12 hours, 2 / 3 of the supernatant was taken for centrifugation, and washed with deionized water for 3 times to obtain a two-dimensional layered SrCuSi 4 o 10 single crystal. Finally dispersed in 3ml deionized water.
[0027] (2) Disperse 0.2g of PVA powder in 4ml of deionized water and stir at 80°C for 2h to dissolve the powder.
[0028] (3) Mix 4ml of PVA aqueous solution and 3ml of SrCuSi 4 o 10 Mix the aqueous solution evenly, pour it into a watch glass with a smooth surface, and place it horizontally in a drying oven to dry for two days to obtain a flat and dry PVA film.
[0029] (4) Select the part with uniform thickness as a saturable absorber device. Using...
Embodiment 2
[0031] This example illustrates how to prepare a saturable absorber of two-dimensional crystals of SrCuSi4O10 supported in the polymer polymethylmethacrylate (PMMA).
[0032] (1) 0.15g of SrCuSi 4 o 10 The crystals were added to 20ml hydrochloric acid solution of 3mol / L, ultrasonically treated, and left to stand for 12 hours, 2 / 3 of the supernatant was taken for centrifugation, and washed with deionized water for 3 times to obtain a two-dimensional layered SrCuSi 4 o 10 single crystal. Finally dispersed in 3ml of N-vinylpyrrolidone (NVP).
[0033] (2) Disperse 0.2g PMMA powder in 4ml NVP, stir for 2h to dissolve the powder, and then mix with (1) obtained SrCuSi 4 o 10 The NVP solution was mixed.
[0034] (3) Spin-coat the solution obtained in (2) on a glass sheet with a thickness of about 0.2 mm at a speed of 1000 rpm, and place it horizontally in a drying oven at 90 ° C for 24 hours under 0.5 MPa pressure to make the solvent completely Volatilize to get a flat and dry ...
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