Preparation method of silver-copper-oxide electrical contact material

A technology of oxide electricity and contact materials, applied in the direction of circuits, electric switches, electrical components, etc., can solve the problem of affecting the comprehensive performance and service life of contact materials, the reduction of electrical conductivity and processing performance of contact materials, and the difficulty of controlling process parameters etc. to achieve the effects of saving preparation cost, improving machinability, wear resistance and fusion welding resistance

Active Publication Date: 2015-12-02
XI'AN POLYTECHNIC UNIVERSITY
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  • Summary
  • Abstract
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  • Application Information

AI Technical Summary

Problems solved by technology

Although the electrical conductivity of the electrical contact materials prepared by these methods is relatively good, most of them have the disadvantages of high cost, complicated process parameters, difficult to control, and long process cycle, making it difficult to realize industrial production and application.
[0005] Especially in the production process of electrical contact materials, a large amount of silver will be used, which will cause an increase in the preparation cost
However, in the existing technology, if the silver content in the preparation process of the electrical contact material is reduced, the electrical conductivity and processing performance of the contact material will also be reduced, which will eventually affect the overall performance and service life of the contact material.
[0006] As far as the existing technology is concerned, there is no method on the market that uses cheap metal copper to replace part of the precious metal silver, and at the same time adds oxides to prepare electrical contact materials

Method used

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Examples

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Effect test

preparation example Construction

[0043] A kind of preparation method of silver-copper oxide electrical contact material of the present invention, specifically implement according to the following steps:

[0044] Step 1. Weigh the oxide powder and the grinding ball respectively, and process the oxide powder symmetrically taken by the high-energy ball milling method to obtain the nano-scale oxide powder. Specifically, follow the steps below:

[0045] Step 1.1, weighing the oxide powder and the grinding ball respectively, the mass ratio of the oxide powder and the grinding ball is 1: (5-30);

[0046] Oxide powder adopts SnO 2 powder, ZnO powder, SiO 2 powder, CdO powder, La 2 o 3 powder or CuO powder;

[0047] Step 1.2, first add the oxide powder weighed in step 1.1 together with the balls into the ball milling tank, then add absolute ethanol to the ball milling tank, add 2.8ml to 3.8ml of absolute ethanol for each gram of oxide powder, and start the ball milling The tank starts ball milling treatment, and ...

Embodiment 1

[0068] Weigh the SnO 2 Powder and Stainless Steel Grinding Balls, SnO 2 The mass ratio of the powder to the stainless steel grinding ball is 1:5; the weighed SnO 2 The powder is added into the ball milling jar together with stainless steel balls, and then absolute ethanol is added to the ball milling jar, each gram of SnO 2 Add 2.8ml of absolute ethanol to the powder, open the ball mill tank, and get nano SnO after ball milling for 4 hours 2 powder; nano-SnO obtained after ball milling 2 The powder is placed in the air to dry to obtain nano-scale SnO 2 Powder;

[0069] Weigh silver powder, copper powder and nanoscale SnO respectively according to the mass ratio of 90:5:5 2 powder; wherein the average particle size of the silver powder is 45 microns; the silver powder, copper powder, nano-scale SnO 2 Mix the powder evenly to form mixed powder A; weigh stainless steel grinding balls and mixed powder A respectively, the ball-to-material ratio of mixed powder A and stainless...

Embodiment 2

[0072] Weigh ZnO powder and bearing steel grinding balls respectively, the mass ratio of ZnO powder and bearing steel grinding balls is 1:20; first put the weighed ZnO powder and bearing steel grinding balls into the ball milling jar, and then add no Water ethanol, add 3.2ml of absolute ethanol per gram of ZnO powder, open the ball mill tank, and get nano ZnO powder after ball milling for 2 hours; place the nano ZnO powder obtained after ball milling in the air to dry, and get nano ZnO powder;

[0073] Weigh silver powder, copper powder and nano-sized ZnO powder respectively according to the mass ratio of 70:20:10; the average particle size of the silver powder is 65 microns; mix the weighed silver powder, copper powder, and nano-sized ZnO powder evenly, Form the mixed powder A; weigh the bearing steel grinding ball and the mixed powder A respectively, the ball-to-material ratio of the mixed powder A and the bearing steel grinding ball is 1:15; first weigh the bearing steel gri...

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Abstract

The invention discloses a preparation method of a silver-copper-oxide electrical contact material, which comprises the following steps: 1 weighing oxide powder and abrading-ball respectively and processing the weighed oxide powder through the high energy ball milling method to obtain a nanometer level oxide powder; 2 mixing a silver powder, a copper powder and a nanometer level oxide powder obtained from step 1 to obtain a mixed powder A, and conducting mechanical alloyage surface treatment to the mixed powder A to obtain a mixed powder B; and 3 conducting procedures of annealing, moulding, sintering and extruding to the mixed powder B obtained from step 2 to obtain the silver-copper-oxide electrical contact material. According to the preparation method of the silver-copper-oxide electrical contact material, the cheap metal copper is used to substitute partial precious metals silver; at the same time, oxide is added to prepare the electrical contact material; in this way, not only the preparation cost is low; the obtained electrical contact material has good conductive performance and long service life.

Description

technical field [0001] The invention belongs to the technical field of preparation methods of composite materials, and in particular relates to a preparation method of a silver-copper oxide electrical contact material. Background technique [0002] The existing preparation methods of silver-based electrical contact materials are mainly divided into traditional processes and new processes that are beneficial to improve the performance of contacts. [0003] The traditional process can be roughly divided into two types, namely: general powder metallurgy method (traditional powder metallurgy method, reaction spray method, mechanical alloying method, reaction synthesis method) and internal oxidation method (alloy internal oxidation method, pre-oxidized alloy method) However, most of the conventional techniques have the problems of poor overall performance and short service life of the prepared electrical contact materials. [0004] In recent years, new processes that are conduci...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F3/16B22F9/04H01H11/04
Inventor 王俊勃思芳刘松涛杨敏鸽贺辛亥付翀曹风郭天福
Owner XI'AN POLYTECHNIC UNIVERSITY
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