Preparation method of wheat straw and hydrotalcite composite material capable of adsorbing cobalt ions in electroplating water
A composite material, wheat straw technology, applied in adsorption water/sewage treatment, chemical instruments and methods, water/sludge/sewage treatment, etc., to achieve outstanding effect of regeneration and recycling
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Embodiment 1
[0016] Harvest the wheat straw, wash it with tap water, and dry it.
[0017] Dissolve ammonia water, ammonium chloride, urea, and magnesium chloride in deionized water, the concentration of ammonia water is 3g / L, the concentration of ammonium chloride is 3g / L, the concentration of urea is 6g / L, and the concentration of magnesium chloride is 1g / L to obtain an ammoniated solution .
[0018] Put 50 g of washed wheat straw in 500 mL of ammoniated solution, place it at 30° C. for 30 minutes, rinse and dry to obtain ammoniated wheat straw.
[0019] Dissolve acrylic acid and azobisisobutyronitrile in deionized water, the mass concentration of acrylic acid is 20%, and the mass concentration of azobisisobutyronitrile is 0.3%, to obtain acrylic acid / azobisisobutyronitrile mixed aqueous solution.
[0020] Put 100g of hydrotalcite in 500mL of acrylic acid / azobisisobutyronitrile mixed aqueous solution, stir for 1 hour, filter, dry at 90°C for 3 hours, cool, wash with deionized water, and ...
Embodiment 2
[0025] Harvest the wheat straw, wash it with tap water, and dry it.
[0026] Dissolve ammonia water, ammonium chloride, urea, and magnesium chloride in deionized water, the concentration of ammonia water is 6g / L, the concentration of ammonium chloride is 6g / L, the concentration of urea is 3g / L, and the concentration of magnesium chloride is 3g / L to obtain an ammoniated solution .
[0027] Put 50 g of washed wheat straw in 500 mL of ammoniated solution, place it at 30° C. for 30 minutes, rinse and dry to obtain ammoniated wheat straw.
[0028] Dissolve acrylic acid and azobisisobutyronitrile in deionized water, the mass concentration of acrylic acid is 30%, and the mass concentration of azobisisobutyronitrile is 0.1%, to obtain acrylic acid / azobisisobutyronitrile mixed aqueous solution.
[0029] Put 100 g of hydrotalcite in 2000 mL of acrylic acid / azobisisobutyronitrile mixed aqueous solution, stir for 1 hour, filter, dry at 90°C for 6 hours, cool, wash with deionized water, a...
Embodiment 3
[0034] Harvest the wheat straw, wash it with tap water, and dry it.
[0035] Dissolve ammonia water, ammonium chloride, urea, and magnesium chloride in deionized water, the concentration of ammonia water is 4g / L, the concentration of ammonium chloride is 5g / L, the concentration of urea is 5g / L, and the concentration of magnesium chloride is 2g / L to obtain an ammoniated solution .
[0036] Put 100 g of washed wheat straw into 500 mL of ammoniated solution, place it at 30° C. for 30 minutes, rinse and dry to obtain ammoniated wheat straw.
[0037] Dissolve acrylic acid and azobisisobutyronitrile in deionized water, the mass concentration of acrylic acid is 25%, and the mass concentration of azobisisobutyronitrile is 0.2%, to obtain acrylic acid / azobisisobutyronitrile mixed aqueous solution.
[0038] Put 100 g of hydrotalcite in 1000 mL of acrylic acid / azobisisobutyronitrile mixed aqueous solution, stir for 1 hour, filter, dry at 90°C for 4 hours, cool, wash with deionized water, ...
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