Method for preparing carbon nano tube by means of nickel chloride catalyst
A technology of carbon nanotubes and nickel chloride, which is applied in the field of chemical reactions, can solve problems such as expensive equipment, high raw material prices, and complicated processes, and achieve easy-to-operate, controllable, and low-cost effects
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Embodiment 1
[0021] 3 grams of glucose, 3 grams of melamine, 3 grams of nickel chloride and 5 milliliters of distilled water were mixed and ground into a uniform mixture, and the above mixture was dried at 80 degrees Celsius for 12 hours to obtain a green solid; the above green solid was ground into powder and then transferred to In the high-temperature tube furnace, the temperature was raised to 700 degrees Celsius in flowing nitrogen, and maintained at 700 degrees Celsius for 4 hours to obtain a black solid; the above-mentioned black solid was cooled to room temperature, transferred to a glass beaker, and added 50 milliliters of HCl with a content of 10% ( mass percent) hydrochloric acid solution, stirred and dissolved for 6 hours; after the above-mentioned solid matter washed with hydrochloric acid was suction-filtered with a microporous membrane, washed with 2000 milliliters of distilled water to neutrality, and then rinsed with 50 milliliters of acetone, the obtained solid The product ...
Embodiment 2
[0023] 3 grams of glucose, 3 grams of melamine, 3 grams of nickel chloride and 5 milliliters of distilled water were mixed and ground into a uniform mixture, and the above mixture was dried at 80 degrees Celsius for 12 hours to obtain a green solid; the above green solid was ground into powder and then transferred to In the high-temperature tube furnace, the temperature was raised to 750 degrees Celsius in flowing nitrogen, and maintained at 750 degrees Celsius for 4 hours to obtain a black solid; the above-mentioned black solid was cooled to room temperature, transferred to a glass beaker, and added 50 milliliters of HCl with a content of 10% ( mass percent) hydrochloric acid solution, stirred and dissolved for 6 hours; after the above-mentioned solid matter washed with hydrochloric acid was suction-filtered with a microporous membrane, washed with 2000 milliliters of distilled water to neutrality, and then rinsed with 50 milliliters of acetone, the obtained solid The product ...
Embodiment 3
[0025] 3 grams of glucose, 3 grams of melamine, 3 grams of nickel chloride and 5 milliliters of distilled water were mixed and ground into a uniform mixture, and the above mixture was dried at 80 degrees Celsius for 12 hours to obtain a green solid; the above green solid was ground into powder and then transferred to In the high-temperature tube furnace, the temperature was raised to 800 degrees Celsius in flowing nitrogen, and maintained at 800 degrees Celsius for 4 hours to obtain a black solid; the above-mentioned black solid was cooled to room temperature, transferred to a glass beaker, and 50 milliliters of HCl was added with a content of 10% ( mass percent) hydrochloric acid solution, stirred and dissolved for 6 hours; after the above-mentioned solid matter washed with hydrochloric acid was suction-filtered with a microporous membrane, washed with 2000 milliliters of distilled water to neutrality, and then rinsed with 50 milliliters of acetone, the obtained solid The prod...
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