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Hard anti-reflection composite film type optical window and preparation method thereof

An optical window and composite film technology, applied in optics, optical components, ion implantation coating, etc., can solve the problems of mismatching thermal expansion coefficient and poor adhesion between diamond-like carbon film and optical window, and improve the resistance to sand erosion and rain. Corrosion ability, bonding force enhancement, the effect of improving transmittance

Active Publication Date: 2016-02-03
LUOYANG INST OF ELECTRO OPTICAL EQUIP OF AVIC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The purpose of the present invention is to provide a hard anti-reflection composite film optical window, thereby solving the problems of the thermal expansion coefficient mismatch and poor adhesion between the diamond-like film and the optical window in the prior art, and realizing efficient anti-reflection for the optical window. And improve the anti-sand erosion and rain erosion ability of the optical window surface

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] The optical window of the hard anti-reflection composite film in this embodiment has a Sub|HL film system, wherein Sub is the substrate of the optical window, H is the germanium bonding layer, and L is the diamond-like film.

[0030] The preparation method of the hard anti-reflection composite film optical window of the present embodiment comprises the following steps:

[0031] (1) Vacuum evaporation method is used to plate a germanium bonding layer on the ZnS optical window substrate

[0032] 1) Scrub the base of the optical window with a mixture of alcohol and ether (the volume ratio of alcohol and ether is 1:1) to remove surface impurities, oil stains and auxiliary materials; then place the base of the optical window in a vacuum chamber and evacuate to 1×10 -2 Pa, heat the base of the optical window to 180°C and keep it warm for 1 hour;

[0033] 2) The optical window substrate is bombarded with an RF radio frequency source for 6 minutes;

[0034] 3) Evaporate germa...

Embodiment 2

[0041] The optical window of the hard anti-reflection composite film in this embodiment has a Sub|HL film system, wherein Sub is the substrate of the optical window, H is the germanium bonding layer, and L is the diamond-like film.

[0042] The preparation method of the hard anti-reflection composite film optical window of the present embodiment comprises the following steps:

[0043] (1) Vacuum evaporation method is used to plate a germanium bonding layer on the ZnS optical window substrate

[0044] 1) Scrub the base of the optical window with a mixture of alcohol and ether (the volume ratio of alcohol and ether is 1:1) to remove surface impurities, oil stains and auxiliary materials; then place the base of the optical window in a vacuum chamber and evacuate to 1×10 -2 Pa, heat the optical window substrate to 200°C and keep it warm for 1 hour;

[0045] 2) The optical window substrate is bombarded with an RF radio frequency source for 5 minutes;

[0046] 3) Evaporate germani...

Embodiment 3

[0053] The optical window of the hard anti-reflection composite film in this embodiment has a Sub|HL film system, wherein Sub is the substrate of the optical window, H is the germanium bonding layer, and L is the diamond-like film.

[0054] The preparation method of the hard anti-reflection composite film optical window of the present embodiment comprises the following steps:

[0055] (1) Vacuum evaporation method is used to plate a germanium bonding layer on the ZnSe optical window substrate

[0056] 1) Scrub the base of the optical window with a mixture of alcohol and ether (the volume ratio of alcohol and ether is 1:1) to remove surface impurities, oil stains and auxiliary materials; then place the base of the optical window in a vacuum chamber and evacuate to 1×10 -2 Pa, heat the optical window substrate to 160°C and keep it warm for 1 hour;

[0057] 2) The optical window substrate is bombarded with an RF radio frequency source for 6 minutes;

[0058] 3) Evaporate german...

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Abstract

The invention discloses a hard anti-reflection composite film type optical window and a preparation method thereof, and belongs to the technical field of manufacturing of optical part films. The optical window is provided with a Sub / HL film system, wherein Sub is a base of the optical window; H is a germanium combined layer; L is a diamond-like film. According to the hard anti-reflection composite film type optical window, the germanium combined layer is introduced between the optical window and the diamond-like film, thus the problems of mismatching of the diamond-like film and a thermal expansions system of the optical window and poor adhesiveness can be solved, and the deposition of the diamond-like film on the surface of the optical window can be achieved; the combined layer and the diamond-like film are combined, so that the transmissivity of the optical window can be improved, the resistance of the surface of the window to sand corrosion and rain corrosion can be improved, and meanwhile, the environmental reliability of a film layer on the surface of the optical window can be improved, and as a result, the service life of the optical window can be prolonged.

Description

technical field [0001] The invention belongs to the technical field of thin film manufacturing of optical parts, and in particular relates to a hard antireflection composite film optical window and a preparation method thereof. Background technique [0002] In the field application environment such as sea surface and space, the optical window should not only have good optical characteristics, but also have high hardness, corrosion resistance, impact resistance and other characteristics. Common optical window materials can be ZnS, ZnSe, Si, SiO 2 , AS 2 S 3 , KCl, CaF 2 etc. Its shape can be flat plate, spherical crown and other shapes. The operating environment of the optical window is harsh, and it is often eroded by wind, sand and rain. The surface of the optical window eroded by rain and sand will cause serious light scattering to the incident light, which will inevitably reduce the transmittance of the optical window, and seriously cause the optical system to lose T...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C14/18C23C14/24G02B1/115G02B1/14
Inventor 吴晓鸣王一坚刘佳琳孙红晓陈小鹏
Owner LUOYANG INST OF ELECTRO OPTICAL EQUIP OF AVIC
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