Graphite/silicon carbide composite material and preparation method thereof
A technology of composite materials and silicon carbide, which is applied in the field of materials, can solve the problems of destroying the original shape of whisker materials and difficult to obtain high mechanical strength characteristics, and achieve the effects of excellent thermal shock resistance, high hardness and high elastic modulus
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[0023] The invention provides a kind of preparation method of graphite / silicon carbide composite material, it comprises the following steps:
[0024] S1, mixing magnesium borate whiskers, foaming agent and water in a foaming machine to obtain a foamy first mixture, wherein the weight portion of magnesium borate whiskers is 0.05 to 1.2, and the weight portion of foaming agent is 0.1~0.3, the weight part of water is 3~10;
[0025] S2, mixing graphite and silicon carbide to obtain a second mixture, wherein the weight ratio of graphite to silicon carbide is 1:(1-5);
[0026] S3, uniformly mixing the first mixture and the second mixture to obtain a third mixture, wherein the weight part of the second mixture is 10;
[0027] S4, performing press molding on the third mixture, and sintering at high temperature to obtain the graphite / silicon carbide composite material.
[0028] In step S1, the time for mixing the magnesium borate whiskers, foaming agent and water in the foaming machi...
Embodiment 1
[0038] This embodiment uses high-purity raw materials.
[0039] 0.2 parts by weight of magnesium borate whiskers, 0.2 parts by weight of sodium dodecylbenzenesulfonate and 5 parts by weight of water were mixed in a foaming machine to form a foamy first mixture. Graphite and silicon carbide were mixed in a weight ratio of 1:1 to obtain a second mixture. Mix the first mixture and 10 parts by weight of the second mixture uniformly to obtain a third mixture. After the mixing is completed, the third mixture is press-molded under a pressure of 80 MPa and sintered at a high temperature of 1200 degrees Celsius to obtain the graphite / silicon carbide composite material.
[0040] The obtained graphite / silicon carbide composite material is subjected to a mechanical performance test, and the obtained test results are shown in figure 1 .
Embodiment 2
[0042] This preparation method is basically consistent with the preparation method of Example 1, except that 0.4 parts by weight of magnesium borate whiskers are used.
[0043] The obtained graphite / silicon carbide composite material is subjected to a mechanical performance test, and the obtained test results are shown in figure 1 .
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