Low-viscosity high-transparency self-adhesive organic silicone pouring sealant and preparation method thereof

A silicone potting glue and self-adhesive technology, applied in the field of potting glue, can solve the problems of poor adhesion of the potting glue, increase the production process, high viscosity, achieve good bonding performance and mechanical properties, easy industrial production, Simple preparation method

Inactive Publication Date: 2016-05-18

FOSHAN XINXIANGXING CHEM

3 Cites 9 Cited by

AI-Extracted Technical Summary

Problems solved by technology

Chinese patent CN102382618A discloses a two-component high-strength transparent room temperature curing silicone potting compound, wherein the silicone resin is dissolved with toluene, which increases the production process and reduces production efficiency. The organic solvent toluene can also cause certain effects on the human body damage, pollute the environment, and this potting adhesive has poor adhesion, high v...

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Abstract

The invention discloses a low-viscosity high-transparency self-adhesive organic silicone pouring sealant and a preparation method thereof. The preparation method includes the steps of feeding polydimethylsiloxane with terminal vinyl groups, vinyl MQ silicone resin, polymethylhydrosiloxane, an adhesion promoter, 1-acetenyl-1-cyclohexanol and a Karstedt catalyst into a high-speed dispersing machine, and mixing the components uniformly to prepare the low-viscosity high-transparency self-adhesive organic silicone pouring sealant. The pouring sealant is higher than 96% in light transmittance, is good in flowability, is easy to use, can be cured at normal temperature or under heating conditions, has good adhesion and mechanical performance, and can be widely used in the fields of optical devices, LED chip potting and the like with high requirements on transparency and adhesion strength.

Application Domain

Non-macromolecular adhesive additivesOther chemical processes

Technology Topic

PolymethylhydrosiloxaneChemistry +11

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Examples

Experimental program(5)

Example Embodiment

[0019] Example 1

[0020] 100 parts by mass of vinyl-terminated polydimethylsiloxane with a viscosity of 1000 mPa·s, 20 parts by mass of vinyl MQ silicone resin (vinyl content of 0.5%, M/Q value 0.8), 4.5 parts by mass of viscosity 50mPa·s polymethylhydrogensiloxane, 1.5 parts by mass of vinyltrimethoxysilane, 0.02 parts by mass of 1-ethynyl-1-cyclohexanol and 0.3 parts by mass of platinum content of 4000ppm Castel catalyst were added to the high-speed disperser, Stir for 1 hour to obtain a low-viscosity, high-transparent, self-adhesive silicone potting glue. The performance test showed that the viscosity was 1500 mPa·s, the light transmittance was 97%, and the bonding tensile shear strength (abbreviated as shear strength, the same below) was 1.02 MPa. The detailed results are shown in Table 1.

Example Embodiment

[0021] Example 2

[0022] 100 parts by mass of vinyl-terminated polydimethylsiloxane with a viscosity of 800 mPa·s, 30 parts by mass of vinyl MQ silicone resin (vinyl content of 1%, M/Q value of 1), 5 parts by mass of viscosity 30mPa·s polymethylhydrogensiloxane, 2 parts by mass of vinyltrimethoxysilane, 0.01 parts by mass of 1-ethynyl-1-cyclohexanol and 0.4 parts by mass of platinum content of 2500ppm Castel catalyst were added to the high-speed disperser, Stir for 2h to obtain a low-viscosity, high-transparent, self-adhesive silicone potting glue. The performance test showed that the viscosity was 1800 mPa·s, the light transmittance was 97%, and the shear strength was 1.15 MPa. The detailed results are shown in Table 1.

Example Embodiment

[0023] Example 3

[0024] 100 parts by mass of vinyl-terminated polydimethylsiloxane with a viscosity of 2000 mPa·s, 15 parts by mass of vinyl MQ silicone resin (vinyl content of 6.5%, M/Q value of 1.2), and 7.5 parts by mass of viscosity 150mPa·s polymethylhydrogensiloxane, 1.5 parts by mass of 3-methacryloxypropyltrimethoxysilane, 0.02 parts by mass of 1-ethynyl-1-cyclohexanol and 0.2 parts by mass of platinum with a content of 5000 ppm calories Stir catalyst was added to the high-speed disperser and stirred for 3 hours to obtain a low-viscosity, high-transparent, self-adhesive silicone potting sealant. The performance test showed that the viscosity was 2300 mPa·s, the light transmittance was 98%, and the shear strength was 1.03 MPa. The detailed results are shown in Table 1.

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PUM

Property	Measurement	Unit
Viscosity	1500.0	mPa·s
Viscosity	1800.0	mPa·s
Shear strength	1.15	mPa
tensile		MPa
Particle size		Pa
strength	10

Description & Claims & Application Information

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Ultraviolet ray irradiation device, recording apparatus using the ultraviolet ray irradiation device, and recording method

ActiveUS20080174649A1Low viscosityInking apparatusRadiation pyrometryColor printingColor mixing

Owner:SEIKO EPSON CORP

Preparation of polyurethane curing agent with low free toluene diisocyanate

InactiveCN1424345ALow viscosityGood stabilitySolventHydrocarbons.aliphatic

Owner:SHENZHEN FEIYANG IND CO LTD

Classification and recommendation of technical efficacy words

Low viscosity
Good liquidity

Low-viscosity high-transparency self-adhesive organic silicone pouring sealant and preparation method thereof

AI-Extracted Technical Summary

Problems solved by technology

Abstract

Image

Examples

Example Embodiment

Example Embodiment

Example Embodiment

PUM

Description & Claims & Application Information

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