A method for preparing gelatin from poultry skin and its preparation method
A technology for poultry and gelatin, applied in the field of agricultural product processing, can solve the problems of poor gelatin decolorization effect, cumbersome preparation steps, low yield and the like, and achieves the effects of good application prospect, less energy consumption and high yield
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Embodiment 1
[0027] A kind of method using poultry skin as raw material to prepare gelatin, concrete steps are as follows:
[0028] 1) Poultry skin pretreatment: clean the chicken skin, depilate, cut into small pieces of 3×3 mm, soak in 8% salt water for 2 hours, and wash with water;
[0029] 2) One-time ultrasonic acidification: use acetone as solvent, cover the pretreated chicken skin, add phosphoric acid with a concentration of 10%, adjust the pH to 3-4, the ultrasonic oscillation frequency is 20kHz, and the oscillation time is 2h;
[0030] 3) Alkali washing: add triethylamine to the solution obtained in step 2) to make the pH 10, and soak for 5 hours;
[0031] 4) Secondary ultrasonic acidification: the solution in step 3) is concentrated under reduced pressure and washed with water, adding ethanol twice the weight of chicken skin, adding hydrochloric acid with a concentration of 20%, adjusting the pH to 6-7, and the ultrasonic oscillation frequency to 15kHz. The shaking time is 2h;
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Embodiment 2
[0035] A kind of method using poultry skin as raw material to prepare gelatin, concrete steps are as follows:
[0036] 1) Poultry skin pretreatment: clean the duck skin, depilate, cut into 4×4mm small pieces, soak in 9% salt water for 4 hours, and wash with water;
[0037] 2) One-time ultrasonic acidification: use acetone as solvent, submerge the pretreated duck skin, add phosphoric acid with a concentration of 20%, adjust the pH to 3-4, the ultrasonic oscillation frequency is 25kH, and the oscillation time is 3h;
[0038] 3) Alkali washing: add pyridine to the solution obtained in step 2) to make the pH 11, and soak for 5 hours;
[0039] 4) secondary ultrasonic acidification: the solution in step 3) is concentrated under reduced pressure and then washed with water, adding propanol with 2 times the weight of duck skin, adding hydrochloric acid with a concentration of 20%, adjusting the pH to 6-7, and the ultrasonic oscillation frequency is 15kHz, the oscillation time is 3h; ...
Embodiment 3
[0043] A kind of method using poultry skin as raw material to prepare gelatin, concrete steps are as follows:
[0044] 1) Poultry skin pretreatment: clean the chicken skin, depilate, cut into 5×5mm small pieces, soak in 10% salt water for 5 hours, and wash with water;
[0045]2) One-time ultrasonic acidification: use acetone as solvent, cover the pretreated chicken skin, add phosphoric acid with a concentration of 30%, adjust the pH to 3-4, the ultrasonic oscillation frequency is 20kHz, and the oscillation time is 5h;
[0046] 3) Alkali washing: add KOH to the solution obtained in step 2) to make the pH 12, and soak for 5 hours;
[0047] 4) secondary ultrasonic acidification: the solution in step 3) is concentrated under reduced pressure and washed with water, adding ethylene glycol with a weight twice that of chicken skin, adding hydrochloric acid with a concentration of 20%, adjusting the pH to 6-7, and the ultrasonic oscillation frequency is 15kHz, the oscillation time is ...
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