Flame-retardant insulating composite and preparation method thereof
A technology of insulating composite materials and resin materials, which is applied in the field of insulating composite materials, can solve the problems of easy combustion or ablation, decreased insulation performance, poor insulation performance, etc., and achieves good mechanical properties, guaranteed strength and good compatibility of products Effect
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Embodiment 1
[0018] (1) Add 28g glass fiber to 100g ethanol, stir for 25 minutes; then add 100g isomeric tridecanol polyoxyethylene ether, stir for 1 hour, then remove ethanol to obtain active glass fiber; in 100g unsaturated polyester resin , add 14g 5,5'-bis(triethoxysilyl)-3,3'-bipyridine, 250g N,N-dimethylformamide and 10g pentaerythritol tetraacrylate, stir for 20 minutes, then add 15g hydrogen Magnesium oxide powder and 12 g of antimony trioxide powder were stirred for 2 hours; 15 g of di-n-hexylamine and 18 g of m-aminoacetanilide were added and stirred for 15 minutes; then 40 g of N-acetyl p-aminophenol was added and stirred for 2 hours to obtain a resin material;
[0019] (2) Add 13g of active glass fiber to 100g of resin material, and mix it with a kneader to become the raw material of flame-retardant and insulating composite material; add the raw material of flame-retardant and insulating composite material to a mold preheated at 55°C, and raise the temperature to 60°C. Hold for...
Embodiment 2
[0021] (1) Add 20g of glass fiber to 100g of ethanol, stir for 25 minutes; then add 100g of isomeric tridecanol polyoxyethylene ether, stir for 1 hour, then remove the ethanol to obtain active glass fiber; in 100g of unsaturated polyester resin , add 12g of 5,5'-bis(triethoxysilyl)-3,3'-bipyridine, 200g of N,N-dimethylformamide and 8g of pentaerythritol tetraacrylate, stir for 20 minutes, then add 13g of hydrogen Magnesium oxide powder, 8g antimony trioxide powder, stirred for 2 hours; then added 13g of di-n-hexylamine, 15g of m-aminoacetanilide, stirred for 15 minutes; then added 20g of N-acetyl p-aminophenol, stirred for 2 hours to obtain a resin material;
[0022] (2) Add 12g of active glass fiber to 100g of resin material, and mix it with a kneader to become the raw material of flame-retardant and insulating composite material; add the raw material of flame-retardant and insulating composite material to a mold preheated at 55°C, and heat up to 60°C. Hold for 35 minutes; th...
Embodiment 3
[0024] (1) Add 25g of glass fiber to 100g of ethanol, stir for 25 minutes; then add 100g of isomeric tridecanol polyoxyethylene ether, stir for 1 hour, then remove the ethanol to obtain active glass fiber; in 100g of unsaturated polyester resin , add 13g 5,5'-bis(triethoxysilyl)-3,3'-bipyridine, 220g N,N-dimethylformamide and 9g pentaerythritol tetraacrylate, stir for 20 minutes, then add 14g hydrogen Magnesium oxide powder and 10 g of antimony trioxide powder were stirred for 2 hours; then 14 g of di-n-hexylamine and 16 g of m-aminoacetanilide were added and stirred for 15 minutes; then 30 g of N-acetyl p-aminophenol was added and stirred for 2 hours to obtain a resin material;
[0025] (2) Add 12.5g of active glass fiber to 100g of resin material, and mix it with a kneader to become the raw material of flame-retardant and insulating composite material; add the raw material of flame-retardant and insulating composite material to the mold preheated at 55°C, and heat up to 60°C ...
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