Epitaxial growing method of LED
An epitaxial growth and reaction chamber technology, applied in electrical components, semiconductor/solid-state device manufacturing, circuits, etc., can solve problems such as low luminous efficiency, current crowded N-layer resistance, and uneven current distribution in the light-emitting layer.
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Embodiment 1
[0049] see figure 2 , the present invention uses MOCVD to grow high-brightness GaN-based LED epitaxial wafers. Using high-purity H 2 or high purity N 2 or high purity H 2 and high purity N 2 The mixed gas as the carrier gas, high-purity NH 3 As the N source, the metal-organic source trimethylgallium (TMGa) is used as the gallium source, trimethylindium (TMIn) is used as the indium source, and the N-type dopant is silane (SiH 4 ), trimethylaluminum (TMAl) as the aluminum source, and the P-type dopant as magnesium dicene (CP 2 Mg), the substrate is (001) sapphire, and the reaction pressure is between 70mbar and 900mbar. The specific growth method is as follows:
[0050] A kind of LED epitaxial growth method, see figure 1 , is characterized in that it includes in sequence: processing the substrate, growing a low-temperature buffer layer GaN, growing an undoped GaN layer, growing an N-type GaN layer doped with Si, growing a light-emitting layer, growing a P-type AlGaN lay...
Embodiment 2
[0060] The application examples of the LED epitaxial growth method of the present invention are provided below, and its epitaxial structure can be found in figure 2 , growth method see figure 1 . Using MOCVD to grow high-brightness GaN-based LED epitaxial wafers. Using high-purity H 2 or high purity N 2 or high purity H 2 and high purity N 2 The mixed gas as the carrier gas, high-purity NH 3 As the N source, the metal-organic source trimethylgallium (TMGa) is used as the gallium source, trimethylindium (TMIn) is used as the indium source, and the N-type dopant is silane (SiH 4 ), trimethylaluminum (TMAl) as the aluminum source, and the P-type dopant as magnesium dicene (CP 2 Mg), the substrate is (0001) sapphire, and the reaction pressure is between 70mbar and 900mbar. The specific growth method is as follows:
[0061] Step 101, processing the substrate:
[0062] H at 1000°C-1100°C 2 Under the atmosphere, feed 100L / min-130L / min of H 2 , keep the reaction chamber p...
Embodiment 3
[0086] A conventional LED epitaxial growth method is provided below as a comparative example of the present invention.
[0087] The growth method of conventional LED epitaxy is (see the epitaxial layer structure image 3 ):
[0088] 1. H at 1000°C-1100°C 2 Under the atmosphere, feed 100L / min-130L / min of H 2 , keep the reaction chamber pressure at 100mbar-300mbar, and process the sapphire substrate for 5min-10min.
[0089] 2.1. Lower the temperature to 500°C-600°C, keep the reaction chamber pressure at 300mbar-600mbar, and feed the flow rate at 10000sccm-20000sccm NH 3 (sccm is standard milliliter per minute), TMGa of 50sccm-100sccm, H of 100L / min-130L / min 2 , grow a low-temperature buffer layer GaN with a thickness of 20nm-40nm on a sapphire substrate;
[0090] 2.2. Raise the temperature to 1000°C-1100°C, keep the reaction chamber pressure at 300mbar-600mbar, and feed the flow at 30000sccm-40000sccm NH 3 , 100L / min-130L / min H 2 , keep the temperature stable for 300s-500...
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