Biology base polymer aerogel oil absorption material and preparation method thereof
A bio-based polymer, oil-absorbing material technology, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of low oil quality adsorption capacity, no oil-water selectivity, etc., and achieve excellent compression recovery and high adsorption. Capacity retention, wide-ranging effects
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Embodiment 1
[0040] Add 0.3 parts of propylene glycol alginate to 100 parts of water, heat and stir to dissolve it completely, then add 0.03 parts of hexamethylene diisocyanate, and stir and react at 25°C for 6 hours; pre-freeze the obtained precursor solution at 10°C 12h, and then completely freeze it into a solid at -196°C, and then dry the solid at -20°C for 120h to obtain an airgel; °C for hydrophobic modification for 12 hours to obtain a bio-based polymer airgel super oil-absorbing material.
[0041] The relevant performance test results of the oil-absorbing material are shown in the attached table.
Embodiment 2
[0043] Add 1.0 part of propylene glycol alginate to 100 parts of water, heat and stir to dissolve it completely, then add 0.1 part of hexamethylene diisocyanate, and stir and react at 25°C for 10 hours; pre-freeze the obtained precursor solution at 7°C 12h, and then completely freeze it into a solid at -196°C, and then dry the solid at -50°C for 192h to obtain an airgel; Hydrophobic modification was carried out at 100°C for 9 hours to obtain a bio-based polymer airgel super oil-absorbing material.
[0044] The relevant performance test results of the oil-absorbing material are shown in the attached table.
Embodiment 3
[0046] Add 2.0 parts of propylene glycol alginate to 100 parts of water, heat and stir to dissolve it completely, then add 0.2 parts of hexamethylene diisocyanate, and stir and react at 25°C for 12 hours; pre-freeze the obtained precursor solution at 6°C 12h, and then completely freeze it into a solid at -196°C, and then dry the solid at -20°C for 120h to obtain an airgel; °C for hydrophobic modification for 12 hours to obtain a bio-based polymer airgel super oil-absorbing material.
[0047] The relevant performance test results of the oil-absorbing material are shown in the attached table.
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