Microcapsule double-aqueous-phase purification method of tobacco clove oil, and applications thereof

A clove oil and two-phase technology, which is applied in the field of preparation of cigarette flavors and fragrances, can solve the problems of eugenol deterioration and low purity, and achieve the effects of fine and soft smoke, improved purity and improved quality.

Active Publication Date: 2016-11-23
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

And the main characteristic composition of clove is eugenol, adopts existing preparation method to obtain the content of eugenol the highest can only reach 85%, and its purity is lower
In addition, a good spice extraction method provides the basis for essence purification, while the general volatile oil extraction method, namely steam distillation, requires high temperature, which will cause the heat-sensitive substance eugenol in the essential oil to deteriorate.
Therefore, it is necessary to choose an extraction method that can extract in a low temperature environment and ensure sufficient extraction, and can effectively obtain high-purity eugenol. However, there is currently no better method that can achieve the above effects

Method used

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  • Microcapsule double-aqueous-phase purification method of tobacco clove oil, and applications thereof
  • Microcapsule double-aqueous-phase purification method of tobacco clove oil, and applications thereof
  • Microcapsule double-aqueous-phase purification method of tobacco clove oil, and applications thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Embodiment 1, a microcapsule aqueous two-phase extraction method of clove oil for tobacco is characterized in that the specific steps include:

[0031] (1) Place the dried lilac flower buds in an ultrasonic extraction device, use 45% ethanol aqueous solution as a solvent, add 15 times the extraction solvent of the lilac flower bud quality, and ultrasonicate at a temperature of 55°C and an ultrasonic frequency of 50kHz Extract for 40min to obtain clove extract;

[0032] (2) adopt 0.8 micron ceramic membrane to filter the extract, remove the clove raw material that has been extracted;

[0033] (3) Add 30% food-grade β-cyclodextrin vesicle wall material and 15% food-grade sodium sulfate to the filtered extract, and stir the mixture evenly in a constant temperature water bath at 60°C, usually for about 25 minutes ;

[0034] (4) The mixed solution stirred uniformly in the step (3) is left to stand at normal temperature for 3 hours, and the solvent layer and the dextrin mic...

Embodiment 2

[0037] Embodiment 2, a microcapsule aqueous two-phase extraction method of clove oil for tobacco, is characterized in that the specific steps include:

[0038] (1) Place the dried clove buds in an ultrasonic extraction device, use 40% ethanol aqueous solution as a solvent, add 10 times the mass of clove buds as an extraction solvent, and ultrasonicate at a temperature of 60°C and an ultrasonic frequency of 40kHz Extract for 60min to obtain clove extract;

[0039] (2) adopt 200 mesh sieves to filter the extract, remove the clove raw material that has been extracted;

[0040] (3) Add 50% food-grade β-cyclodextrin vesicle wall material and 12% food-grade sodium chloride to the filtered extract, and stir the mixture in a constant temperature water bath at 50°C for 30 minutes until uniformly mixed;

[0041] (4) The mixed solution stirred uniformly in the step (3) is left to stand at normal temperature for 3 hours, and the solvent layer and the dextrin microcapsule layer are obtain...

Embodiment 3

[0044] Embodiment 3, a microcapsule aqueous two-phase extraction method of clove oil for tobacco, is characterized in that the specific steps include:

[0045] (1) Place the dried clove buds in an ultrasonic extraction device, use 50% ethanol aqueous solution as a solvent, add 15 times the mass of clove buds as an extraction solvent, and ultrasonicate at a temperature of 40°C and an ultrasonic frequency of 70kHz Extract for 30min to obtain clove extract;

[0046] (2) Adopt disc centrifuge to filter extract, remove the clove raw material that has been extracted;

[0047] (3) Add 35% food-grade α-cyclodextrin vesicle wall material and 20% food-grade sodium hydroxide to the filtered extract, and stir the mixture in a constant temperature water bath at 30°C for 15 minutes until uniformly mixed;

[0048] (4) The mixed solution stirred uniformly in the step (3) is left to stand at normal temperature for 3 hours, and the solvent layer and the dextrin microcapsule layer are obtained ...

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Abstract

The invention provides a microcapsule double-aqueous-phase extraction method of tobacco clove oil, and applications thereof. The extraction method comprises the following steps: putting cloves into an ultrasonic extraction device, performing ultrasonic extraction by adopting an ethanol water solution as a solvent to obtain a clove extracting liquid, filtering, and adding a cyclodextrin capsule wall material and inorganic salt or inorganic base, evenly stirring and standing and layering; filtering and separating a cyclodextrin microcapsule layer, adding absolute ethanol into the cyclodextrin microcapsule layer and stirring for 30-60 min, and releasing a capsule core; and then filtering and separating the mixed solution to obtain an ethanol layer, and performing decompression distillation until no ethanol is distilled, thus obtaining the tobacco clove oil. The purification method is simple, mild in conditions, and environment-friendly, the purified clove oil selectively retains the characteristic component eugenol of cloves, another two main components, eugenol acetate and caryophyllene, obtained through common vapor distillation can be removed, the invention provides a method for separating and purifying eugenol from clove oil, and the eugenol is used for covering up miscellaneous gas in a cigarette and improving the aroma quality.

Description

technical field [0001] The invention relates to a method for preparing cigarette essence and fragrance, in particular to a microcapsule aqueous two-phase purification method and application of clove oil for cigarettes. Background technique [0002] Clove is an evergreen tree belonging to the genus Myrtaceae. Clove oil has a special and strong spicy aroma, and is widely used in food additives, tobacco, flavoring agents and other fields. Clove oil is an important raw material for blending spicy and sweet aromas in tobacco flavors, and can enhance the pleasant flavor of tobacco. [0003] Generally, clove oil is prepared by steam distillation, but when clove oil is extracted by conventional steam distillation, since the specific gravity of clove oil is close to that of water, the collected volatile oil and water cannot be separated well, so it is generally necessary to use organic solvents such as petroleum ether Carry out further extraction, extraction process is complicated, ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24B15/26A24B3/12
CPCA24B3/12A24B15/26
Inventor 王萍熊国玺王娜喻世涛苗丽坤
Owner HUBEI CHINA TOBACCO IND
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