Magnesium-lithium alloy used for sand mold casting and preparing method of magnesium-lithium alloy
A magnesium-lithium alloy and sand casting technology, applied in the field of magnesium alloys and their preparation, can solve the problems of limited strength improvement of magnesium-lithium alloys, and achieve the effects of reducing shrinkage defects, high thermal stability and improving fluidity
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[0038] The invention also provides a preparation method of the magnesium-lithium alloy suitable for sand casting. The preparation method includes a smelting step and a heat treatment step.
[0039] The smelting step specifically adopts the following methods:
[0040] A1. Baking material: Weigh pure Mg, pure Al, pure Zn, Mg-Nd master alloy, Mg-Ce master alloy, Al-Ti master alloy, Al- For Ti–C master alloy and Li rod, preheat all the above raw materials at 180°C to 250°C for 3 hours respectively;
[0041] A2. Molten magnesium: add the dried pure Mg into a lithium salt protection flux and put it into a crucible resistance furnace to melt to form a magnesium liquid;
[0042] A3. Adding Al, Zn, Nd, Ce, Ti and C: When the temperature of the magnesium liquid reaches 690°C to 730°C, add pure Al to the magnesium liquid, and after the pure Al is melted, the melt When the temperature rises to 700°C-730°C, pure Zn is added. After the pure Zn is melted, when the melt temperature rises to...
Embodiment 1
[0055] This embodiment provides a magnesium-lithium alloy suitable for sand casting, its components and mass percentages are: 3wt.% Li, 7wt.% Al, 3.5wt.% Zn, 0.5wt.% Nd, 3wt.% Ce, 0.2wt.% Ti, 0.005wt.% C, the total amount of impurity elements Si, Fe, Cu and Ni is less than 0.02wt.%, and the balance is Mg.
[0056] The preparation method of the magnesium-lithium alloy includes two process steps of smelting and subsequent heat treatment.
[0057] Among them, the previous smelting process is in SF 6 and CO 2 Under the condition of mixed gas protection, the steps are as follows:
[0058] (1) Baking material: Weigh pure Mg, pure Al, pure Zn, Mg-30Nd master alloy, Mg-30Ce master alloy, Al-5Ti master alloy, Al -5Ti-0.5C master alloy and Li rod, weigh lithium salt protective flux and 4% refining flux according to the mass of the prepared alloy, and then preheat all the above-mentioned raw materials at 180° C. for 3 hours; the lithium The salt protection flux is formed by mixing Li...
Embodiment 2
[0069]This embodiment provides a magnesium-lithium alloy suitable for sand casting, and its components and mass percentages are: 10wt.% Li, 2wt.% Al, 0.5wt.% Zn, 3wt.% Nd, 0.5wt.% Ce, 0.05wt.% Ti, 0.05wt.% C, the total amount of impurity elements Si, Fe, Cu and Ni is less than 0.02wt.%, and the balance is Mg.
[0070] The preparation method of the magnesium-lithium alloy includes two process steps of smelting and subsequent heat treatment.
[0071] Among them, the previous smelting process is in SF 6 and CO 2 Under the condition of mixed gas protection, the steps are as follows:
[0072] (1) Baking material: Weigh pure Mg, pure Al, pure Zn, Mg-90Nd master alloy, Mg-20Ce master alloy, Al-2Ti master alloy, Al -2Ti-1C master alloy and Li rod, weigh lithium salt protective flux and 4% refining flux according to the mass of the prepared alloy, and then preheat all the above-mentioned raw materials at 250° C. for 3 hours; the lithium salt The protective flux is composed of LiCl ...
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