Unlock instant, AI-driven research and patent intelligence for your innovation.

A kind of copper ion rapid detection test paper and preparation method thereof

A technology of copper ion detection and test paper, which is applied in the direction of analyzing the material through chemical reaction and analyzing the material through observing the influence of the chemical indicator, so as to achieve the effect of simple production, convenient use and high cost

Inactive Publication Date: 2019-07-16
HENAN UNIV OF URBAN CONSTR
View PDF3 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In recent years, based on naked-eye visual detection of Cu 2+ There have been many reports on the probe, but it can be applied to test paper to detect Cu in environmental water with naked eyes. 2+ fewer probes

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Step 1), prepare the dipping solution. Dissolve 0.8g of soluble starch in hot water (around 50°C), dilute to 100ml, and prepare impregnating solution A; dissolve 1.5g of salicylaldehyde-8-quinolinyloxyacetylhydrazone in DMSO, and dilute to volume to 100ml to prepare impregnation solution B;

[0025] Step 2), fully soak the filter paper strip in the prepared soaking solution A for 5 minutes, take it out, and dry it at room temperature; then fully soak it in the soaking solution B for 2 minutes, take it out, and dry it at room temperature;

[0026] Step 3), cut the dried filter paper block into a certain size, and obtain the copper ion detection test strip;

[0027] Step 4), the Cu 2+ Concentrations were 1×10 -2 g / L, 5×10 -3 g / L, 1×10 -3 g / L, 5×10 -4 g / L, 1×10 -4 Dip and drop the g / L sample on the test paper, let it stand for 1 minute, and record the color development result. If the test paper shows yellow, it is a positive detection. If the test paper does not dev...

Embodiment 2

[0029] Step 1), prepare the dipping solution. Dissolve 0.5g of soluble starch in hot water, dilute to 100ml, and prepare impregnation solution A; dissolve 1g of salicylaldehyde-8-quinolinyloxyacetylhydrazone in DMF, and dilute to 100ml to prepare impregnation solution B;

[0030] Step 2), fully soak the filter paper strip in the prepared soaking solution A for 5 minutes, take it out, and dry it at room temperature; then fully soak it in the soaking solution B for 2 minutes, take it out, and dry it at room temperature;

[0031] Step 3), cut the dried filter paper block into a certain size, and obtain the copper ion detection test strip;

[0032] Step 4), the Cu 2+ Concentrations were 1×10 -2 g / L, 5×10 -3 g / L, 1×10 -3 g / L, 5×10 -4 g / L, 1×10 -4 Dip and drop the g / L sample on the test paper, let it stand for 1 minute, and record the color development result. If the test paper shows yellow, it is a positive detection. If the test paper does not develop color or it is difficu...

Embodiment 3

[0034] Step 1), prepare the dipping solution. Dissolve 0.1g of soluble starch in hot water, dilute to 100ml, and prepare impregnation solution A; dissolve 0.1g of salicylaldehyde-8-quinolinyloxyacetylhydrazone in acetonitrile, and dilute to 100ml to prepare impregnation solution A. Liquid B;

[0035] Step 2), fully soak the filter paper strip in the prepared soaking solution A for 5 minutes, take it out, and dry it at room temperature; then fully soak it in the soaking solution B for 2 minutes, take it out, and dry it at room temperature;

[0036] Step 3), cut the dried filter paper block into a certain size, and obtain the copper ion detection test strip;

[0037]Step 4), the Cu 2+ Concentrations were 1×10 -2 g / L, 5×10 -3 g / L, 1×10 -3 g / L, 5×10 -4 g / L, 1×10 -4 Dip and drop the g / L sample on the test paper, let it stand for 1 minute, and record the color development result. If the test paper shows yellow, it is a positive detection. If the test paper does not develop co...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses copper ion quick detection test paper and a preparation method thereof. The copper ion quick detection test paper is prepared by sequentially soaking filter paper in soaking liquid A and soaking liquid B, taking the filter paper out and drying the same, wherein the soaking A liquid is soluble starch water solution of 1-10g / L in concentration, and the soaking liquid B is salicylaldehyde-8-quinolinoxyacetylhydrazone. The copper ion quick detection test paper is simple to make, low in cost, convenient to use, needless of professional personnel to operate and suitable for quick on-site detection of copper content, especially water body copper ion content detection.

Description

technical field [0001] The invention belongs to the technical field of rapid detection and analysis, and in particular relates to a copper ion rapid detection test paper using salicylaldehyde acetal-8-quinolinyloxyacetylhydrazone as a color developing agent and a preparation method thereof. Background technique [0002] Copper is a non-ferrous metal closely related to human beings, and is widely used in electrical industry, construction, machinery, chemical industry, medicine, pesticide and other fields. In the human body, copper is the most abundant transition metal element after iron and zinc, and it plays a vital role in many physiological processes. However, when copper is present in excess in the body, it disrupts cellular homeostasis, leading to neurodegenerative diseases such as Alzheimer's disease, Menkes' disease, Wilson's disease, and others. However, in industrial production such as mining, copper smelting, processing, and electroplating, a large amount of copper...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): G01N21/78
CPCG01N21/78
Inventor 李霞李银峰刘小华刘伟赵海鹏
Owner HENAN UNIV OF URBAN CONSTR