Resin-base nonlinear composite material for low temperature environment and preparation method of resin-base nonlinear composite material
A composite material, low temperature environment technology
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Embodiment 1
[0026] The preparation process of resin-based nonlinear composite materials for low temperature environment is as follows:
[0027] (1) First add a weighed functional filler into the flask with a particle size of 10-100nm, then add an appropriate amount of anhydrous ethanol and a silane coupling agent in turn, and stir the above mixture for 2.5 hours with a magnetic stirrer until it is evenly mixed Afterwards, the solution was suction-filtered, put into a drying oven, and dried at about 100°C for 10 hours for later use.
[0028] (2) Add the weighed epoxy resin matrix and the above-mentioned functional fillers into the four-necked flask, and stir the mixed solution with a mixer for about 0.5h, so that the epoxy resin matrix and the functional fillers are fully mixed evenly.
[0029] (3) Add the weighed toughening agent and curing agent in sequence to the above mixed solution, and stir the mixture with a mixer for 40 minutes until the mixture becomes transparent without bubbles....
Embodiment 2
[0033] The preparation process of resin-based nonlinear composite materials for low temperature environment is as follows:
[0034] (1) First, add a weighed functional filler into the flask with a particle size of 10-100nm, then add an appropriate amount of anhydrous ethanol and a silane coupling agent in turn, and stir the above mixture for 3.5 hours with a magnetic stirrer until it is evenly mixed Afterwards, the solution was suction-filtered, put into a drying oven, and dried at about 100°C for 12 hours for later use.
[0035] (2) Add the weighed epoxy resin matrix and the above-mentioned functional fillers into the four-necked flask, and stir the mixed solution with a mixer for about 1 hour to fully mix the epoxy resin matrix and the functional fillers.
[0036] (3) Add the weighed toughening agent and curing agent in sequence to the above mixed solution, and stir the mixture for 1 hour with a stirrer until the mixture becomes transparent without bubbles.
[0037] (4) Use...
Embodiment 3
[0040] The preparation process of resin-based nonlinear composite materials for low temperature environment is as follows:
[0041] (1) First, add a weighed functional filler into the flask with a particle size of 10-100nm, then add an appropriate amount of anhydrous ethanol and a silane coupling agent in turn, and stir the above mixture for 3 hours with a magnetic stirrer, and wait until it is evenly mixed Suction filter the solution, put it in a drying oven, and dry it at about 100°C for 11 hours for later use.
[0042] (2) Add the weighed epoxy resin matrix and the above-mentioned functional fillers into the four-necked flask, and stir the mixed solution with a mixer for about 50 minutes to fully mix the epoxy resin matrix and the functional fillers.
[0043] (3) Add the weighed toughening agent and curing agent in sequence to the above mixed solution, and stir the mixture with a mixer for 50 minutes until the mixture becomes transparent without bubbles.
[0044] (4) Use a...
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