Hydrophobic heat-insulation coating and preparation method therof
A heat-insulating coating and hydrophobic technology, applied in the direction of chemical instruments and methods, coatings, fibrous fillers, etc., can solve the problems of ordinary exterior wall emulsion paints such as water resistance, insufficient weather resistance, and damage to the beauty of buildings, and achieve low prices , cost reduction effect
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[0121] Example 1
[0122] 1.TiO 2 Preparation of coated hollow glass beads
[0123] TiO 2 The preparation process of the coated hollow glass beads is as follows:
[0124] (1) Measure 30ml of absolute ethanol and 10ml of butyl titanate into a three-necked flask, at a temperature of 28°C, at a speed of 1800 rpm, stirring for 10 minutes until uniform;
[0125] (2) Add 3ml of glacial acetic acid to the three-necked flask, stir evenly, add 10ml of hollow microbeads, at a temperature of 28℃, at a speed of 1800 rpm, stirring for 20 minutes until uniform;
[0126] (3) Mix 30ml of absolute ethanol and 3ml of water in a beaker and add them to the separatory funnel. Under the condition of a temperature of 28°C, slowly drip into the three-necked flask for 18 minutes;
[0127] (4) Stir and react for 1 hour at a speed of 1800 revolutions / min;
[0128] (5) After standing for 24-48h, put the product in an oven at 100℃ for drying;
[0129] (6) After drying, place the product in a calcining furnace at a tem...
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[0142] Example 2
[0143] Under the condition that other raw materials remain unchanged, the influence of emulsion on the performance of hydrophobic heat insulation coating is investigated, as shown in Table 5:
[0144] Table 5 Effect of emulsion on coating performance
[0145]
[0146] It can be seen from Table 5 that the thermal insulation coating prepared by the silicone-acrylic emulsion is not only higher than the other two products in conventional performance, but also better than the coatings prepared by the other two emulsions. It can be concluded that the selection of silicone-acrylic emulsion in thermal insulation functional coatings can greatly improve the thermal insulation performance, paint film hardness, adhesion and other properties of the coating.
Example Embodiment
[0147] Example 3
[0148] Under the condition of ensuring that other raw materials remain unchanged, the effect of defoamers on the performance of hydrophobic heat insulation coatings is investigated, as shown in Table 6:
[0149] Table 6 Comparison of defoaming effects of defoamers
[0150]
[0151] Through experiments, when only silicone defoamers are used, the defoaming effect of the coating is not ideal. Only by continuing to increase the defoamer can the coating be completely defoamed. Similarly, when only mineral oil defoamers are used, the defoaming effect of the coating is not ideal. Through the comprehensive use of the two defoamers, the coating has achieved perfect defoaming results under the premise of less defoamer dosage. Therefore, the present invention selects the combined use of silicone defoamer and mineral oil defoamer (1:1) (weight ratio).
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