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Graphene organic silicon rubber composite material and preparation method thereof

A technology of silicone rubber and composite materials, applied in the direction of heat exchange materials, chemical instruments and methods, etc., can solve problems such as poor thermal conductivity, achieve improved thermal conductivity, excellent resistance to ultraviolet rays and nuclear radiation, and improve thermal conductivity sexual effect

Inactive Publication Date: 2017-03-29
德阳中碳新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this patent is only suitable for use in the biological living environment covered by the atmosphere, and has certain limitations.
However, the use in special environments such as high temperature and high humidity, high radiation vacuum weightlessness, high radiation nuclear power, and high energy electromagnetic fields will be limited, and its thermal conductivity is poor.

Method used

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  • Graphene organic silicon rubber composite material and preparation method thereof

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Comparison scheme
Effect test

Embodiment 1

[0021] A kind of graphene silicone rubber composite material, comprises the component of following parts by weight:

[0022] 15-39 parts of high phenyl silicone rubber, 1-40 parts of graphene, 55-98 parts of thermal conductive filler, 1-5 parts of silazane, and 1-5 parts of catalyst.

[0023] In this embodiment, the high phenyl silicone rubber is made of tetramethylcyclotetrasiloxane, tetramethyltetraphenylcyclotetrasiloxane, octaphenylcyclotetrasiloxane, divinyltetramethyldi At least two of the siloxanes are polymerized in any proportion under alkaline conditions.

[0024] In this embodiment, the molecular weight of the high-phenyl silicone rubber is 400,000-900,000, the phenyl mass content of the high-phenyl silicone rubber is 30%-70%, and its refractive index is greater than 1.54.

[0025] In this embodiment, the thermally conductive filler is composed of micron alumina compounded with various particle sizes, and the particle size of the micron alumina is 1-400 μm. Furthe...

Embodiment 2

[0029] A kind of graphene silicone rubber composite material, comprises the component of following parts by weight:

[0030] 15 parts of high phenyl silicone rubber, 1 part of graphene, 98 parts of thermally conductive filler, 5 parts of silazane, and 1 part of catalyst.

[0031] In this embodiment, the high phenyl silicone rubber consists of 10 parts of octaphenylcyclotetrasiloxane, 90 parts of tetramethyltetraphenylcyclotetrasiloxane and 2 parts of divinyltetramethyldisiloxane Polymerized under alkaline conditions.

Embodiment 3

[0033] A kind of graphene silicone rubber composite material, comprises the component of following parts by weight:

[0034] 32 parts of high phenyl silicone rubber, 11 parts of graphene, 75 parts of thermally conductive filler, 1 part of silazane, and 4 parts of catalyst.

[0035] In this embodiment, the high phenyl silicone rubber is polymerized by 10 parts of octaphenylcyclotetrasiloxane and 90 parts of tetramethyltetraphenylsiloxane under alkaline conditions.

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Abstract

The invention discloses a graphene organic silicon rubber composite material. The graphene organic silicon rubber composite material comprises, by weight, 15-39 parts of high-phenyl silicone rubber, 1-40 parts of graphene, 55-98 parts of heat-conduction filler, 1-5 parts of silazane and 1-5 parts of catalyst. The invention further provides a preparation method of the graphene organic silicon rubber composite material. The preparation method includes: evenly mixing the graphene, the heat-conduction filler and the silazane, adding the high-phenyl silicone rubber, primarily mixing, adding the catalyst, evenly mixing, performing compression molding, and curing to obtain the graphene organic silicon rubber composite material. The graphene organic silicon rubber composite material and the preparation method thereof have the advantage that the graphene can be stably and evenly distributed in the high-phenyl silicone rubber and a heat-conduction filler interface to form a compact heat-conduction network so as to increase the heat conductivity of the composite material.

Description

technical field [0001] The invention relates to the technical field of thermal interface materials, in particular to a graphene silicone rubber composite material and a preparation method thereof. Background technique [0002] With the further improvement of the operating frequency of electronic devices, the increase of power capacity and the improvement of efficiency and reliability, especially the higher and higher integration level, the devices are required to be smaller and lighter, which will lead to new electronic systems. These changes will bring major challenges to the packaging and assembly of devices, as well as their reliability, heat dissipation and manufacturability. Although the thermal conductivity of various thermal interface materials on the market has increased to 7W / mk, they are still It cannot keep up with the requirements of the current high-speed development of the electronics industry, so it is very necessary to add a layer of thermal interface materia...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L83/04C08L83/07C08K9/06C08K3/04C08K3/22C09K5/14C08G77/20C08G77/04
CPCC08K9/06C08G77/04C08G77/20C08K3/04C08K3/22C08K2003/2227C08K2201/003C08L2201/08C09K5/14C08L83/04
Inventor 夏传军刘伟德翟利伟
Owner 德阳中碳新材料科技有限公司
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