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Oil well cement expanding agent and preparation method thereof,

A technology of oil well cement and expansion agent, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve problems such as poor compatibility, obvious thickening, and inconspicuous cement expansion effect, and achieve stable expansion rate and high compression resistance Effect of strength, good salt resistance and compatibility

Inactive Publication Date: 2017-03-29
CHANGQING GUJING OF CNPC CHUANQING DRILLING ENG +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The purpose of the present invention is to solve the problems that the expansion effect of cement is not obvious under high temperature and high pressure, the compatibility with retarder and fluid loss reducer is poor, and the thickening is obvious.

Method used

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  • Oil well cement expanding agent and preparation method thereof,
  • Oil well cement expanding agent and preparation method thereof,

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Embodiment 1

[0018] In order to solve the problems that the expansion effect of cement is not obvious under high temperature and high pressure, the compatibility with retarder and fluid loss reducer is poor, and the thickening is obvious, this embodiment provides an expansion agent for oil well cement. The expansion agent is a kind of Salt-resistant and compatible inorganic polymer coagulant polyaluminum chloride, the polyaluminum chloride is obtained by reacting aluminum ash, industrial hydrochloric acid and water at a mass ratio of 3:1:3 .

[0019] The cement stone formed by polyaluminum chloride during the hydration process contains both high-reactivity components and low-reactivity components. These formed components will be accompanied by volume expansion, and the reactivity and The effect is different, so it can maintain stable volume expansion in different hydration stages of cement. In the plastic state, the highly reactive components in the expansive material first react with the...

Embodiment 2

[0021] This embodiment provides the preparation method of the oil well cement expansion agent in the above-mentioned embodiment 1, comprising the following steps:

[0022] (1) Prepare aluminum ash, industrial hydrochloric acid and water according to the mass ratio, the mass ratio of aluminum ash, industrial hydrochloric acid and water is 3:1:3;

[0023] (2) Add the aluminum ash prepared in step (1) to the industrial hydrochloric acid, stir continuously and replenish water during the addition process;

[0024] (3) Aluminum ash, industrial hydrochloric acid and water are reacted. During the reaction, the reaction temperature is 80°C-110°C, the reaction time is 6-8h, the pH is controlled at 3.5-4.5, and the aging time is 15-24h, and finally a liquid product is obtained ;

[0025] (4) Filtrate and dry the liquid product obtained in step (3). After the liquid product is filtered and dried, a solid product can be obtained, which is the oil well cement expansion agent to be prepared...

Embodiment 4

[0028] The present embodiment illustrates the oil well cement expansion agent and its preparation method in the present invention in conjunction with specific implementation data:

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Abstract

The invention belongs to the technical field of oil field chemistry, and particularly relates to an oil well cement expanding agent and a preparation method thereof. The oil well cement expanding agent is an oil-gas well cementing set cement anti-gas-channeling additive for the petroleum industry, the oil well cement expanding agent is obtained by that aluminum ash, industrial hydrochloric acid and water in a mass ratio of 3: 1: 3 are allowed to react, so as to obtain poly aluminum chloride. The oil well cement expanding agent disclosed by the invention is an inorganic high polymer coagulant poly aluminum chloride, and is added into cement, the formed set cement has high compressive strength and stable expansion rate at high temperature and high pressure, the thickening time and the compressive strength are not influenced, and the salt resistance and the compatibility are good.

Description

technical field [0001] The invention belongs to the technical field of oilfield chemistry, in particular to an oil well cement expansion agent and a preparation method thereof, which is an anti-gas channeling additive for oil and gas well cementing in the petroleum industry. Background technique [0002] Commonly used oil well cement expansion agents are SEP products, the main components are calcium salts and magnesium salts, brucite, portlandite and ettringite are formed during the hydration process of crystalline substances, accompanied by volume expansion, which compensates for the hardening of cement. shrinkage. There are defects such as poor compatibility with retarder and fluid loss reducer, obvious thickening effect on cement slurry, no expansion when calcium salt is in a plastic state at 75°C, and ineffective use in deep wells. Contents of the invention [0003] The purpose of the invention is to solve the problems that the expansion effect of cement is not obviou...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/03C09K8/473C04B22/12
CPCC09K8/032C04B22/12C09K8/473
Inventor 魏周胜梅明佳饶辰威王大权窦虎清
Owner CHANGQING GUJING OF CNPC CHUANQING DRILLING ENG