A Daye tea extract product liquid detergent and a preparing method thereof
A large-leaf tea and extract technology, applied in chemical instruments and methods, detergent compounding agents, detergent compositions, etc., can solve problems such as water environment pollution and resource waste, and achieve low environmental pollution, odor removal, and good quality. Effects of foaming and foam stabilization properties
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Embodiment 1
[0035] A kind of big leaf tea extract laundry detergent, by weight, consists of the following components:
[0036] 5 parts of oleic acid, 37 parts of tea saponin, 20 parts of sodium dodecylbenzenesulfonate, 10 parts of big leaf tea extract, 1 part of alkali, 30 parts of water.
[0037] Wherein, the preparation method of big leaf tea extract comprises the following steps:
[0038] (1) Take the tea leaves of Taoyuan big leaves for mechanical crushing, add cellulase after crushing, add 0.1g of enzyme for every 1g of big leaf tea, the enzyme activity is 3~4.5U / g, and the enzymatic hydrolysis temperature 45°C, enzymolysis pH value is 4.8, enzymolysis time is not less than 6h; after enzymolysis, mechanically squeeze and filter to obtain filtrate;
[0039] (2) Dilute the filtrate obtained in step (1) 10 times with water, then adopt excessive HP-20 macroporous resin to pass through the column for adsorption, flow rate 1-4BV / h, adsorption time 2-4h, and collect the effluent simultaneo...
Embodiment 2
[0046] A kind of big leaf tea extract laundry detergent, by weight, consists of the following components:
[0047] 15 parts of oleic acid, 30 parts of tea saponin, 30 parts of sodium dodecylbenzenesulfonate, 3 parts of big leaf tea extract, 3 parts of alkali, 40 parts of water.
[0048] Wherein, the preparation method of big leaf tea extract comprises the following steps:
[0049] (1) Take 100g of fresh leaves of Taoyuan Daye and crush them mechanically. After crushing, adjust the pH value to 4.8 with acetic acid buffer, then add 100g of cellulase for enzymolysis for 8 hours, and the enzyme activity is 3-4.5U / g. The temperature is 45°C; after the enzymatic hydrolysis, mechanically press and filter to obtain 85g of filtrate;
[0050] (2) 85g filtrate is adopted 200g AB-8 macroporous resin to pass column adsorption, flow velocity 3BV / h, adsorption time 4h, collect effluent simultaneously;
[0051] (3) The macroporous resin after adsorption is dynamically eluted with ethanol wi...
Embodiment 3
[0056]A kind of big leaf tea extract laundry detergent, by weight, consists of the following components:
[0057] 10 parts of oleic acid, 40 parts of tea saponin, 25 parts of sodium dodecylbenzenesulfonate, 7 parts of big leaf tea extract, 2 parts of alkali, 40 parts of water.
[0058] Wherein, the preparation method of big leaf tea extract comprises the following steps:
[0059] (1) Take 50g of fresh leaves of Taoyuan Daye and crush them mechanically. After crushing, use acetate buffer to adjust the pH value to 5.8, then add 5g of cellulase for enzymolysis for 6 hours, and the enzyme activity is 3-4.5U / g. The temperature is 45°C; after the enzymolysis, mechanically press and filter to obtain 43g of filtrate;
[0060] (2) Adopt 100g of X-5 macroporous resin of 43g filtrate to pass column adsorption, flow velocity 1BV / h, adsorption time 3h, collect effluent simultaneously;
[0061] (3) The macroporous resin after adsorption is dynamically eluted with ethanol with a volume fra...
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