Adsorption treatment method for cationic dye
A cationic dye and adsorption treatment technology, which is applied in the field of adsorption treatment of cationic dyes, can solve the problems of high production cost by chemical method, non-uniform lignin performance, unsatisfactory application performance, etc., and achieves low preparation cost, wide and convenient sources, and easy to use. The effect of industrial production
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Embodiment 1
[0027] The method comprises the steps of:
[0028] (1) Classification of water-soluble lignin and water-insoluble lignin: fully stir 30g of corn alkali lignin and 500ml of distilled water for 20h, then 40KHz ultrasonic assisted treatment for 2min, fully stir, settle and separate, filter, collect settled and filtered solids, vacuum Dry for 20 hours to obtain 17g of water-insoluble lignin.
[0029] (2) Classification of ketone-soluble lignin and ketone-insoluble lignin: fully mix 17g of water-insoluble lignin and 500ml of acetone solvent for 18h, 40KHz ultrasonic assisted treatment for 3min, fully stir, settle and separate, filter, collect settled and filtered solids, and obtain Water-insoluble ketone-insoluble lignin 8g, collect filtrate at the same time, and it is rotary-evaporated and recovered acetone solvent in rotary evaporator, rotary evaporation temperature is 50 ℃, cooling temperature-15 ℃, rotating speed is 80r / min, obtains water-insoluble ketone solution Lignin 9g. ...
Embodiment 2
[0032] The method comprises the steps of:
[0033] (1) Classification of water-soluble lignin and water-insoluble lignin: fully mix 50g of poplar lignin with 500ml of distilled water for 16h, assisted by ultrasonic treatment for 3min, fully stir, settle and separate, filter, collect the sediment and filter, then vacuum dry the solid for 24h to obtain water Insoluble lignin 35g.
[0034] (2) Classification of ketone-soluble lignin and ketone-insoluble lignin: fully mix 35g of water-insoluble lignin and 500ml of methyl ethyl ketone solvent for 20h, assisted by ultrasonic treatment for 2min, stir fully, settle and separate, filter, collect settled and filtered solids, and obtain Water-insoluble ketone-insoluble lignin 15g, collect the filtrate at the same time, and recycle it in a rotary evaporator to recover the acetone solvent. Lignin 20g.
[0035] (3) The products of water-insoluble ketone-insoluble lignin and water-insoluble ketone-soluble lignin were vacuum-dried at 45° C....
Embodiment 3
[0037] The method comprises the steps of:
[0038] (1) Classification of water-soluble lignin and water-insoluble lignin: fully mix 30g of wheatgrass lignin with 1000ml of distilled water for 18h, assisted by ultrasonic treatment for 3min, stir fully, settle and separate, filter, collect and settle, and dry the solid in vacuum for 48h to obtain water Insoluble lignin 18g.
[0039] (2) Classification of ketone-soluble lignin and ketone-insoluble lignin: fully mix 18g of water-insoluble lignin and 1000ml of pentanone solvent for 15h, assisted by ultrasonic treatment for 3min, stir fully, settle and separate, filter, collect the settled and filtered solid, and obtain Water-insoluble ketone-insoluble lignin 7g, collect the filtrate at the same time, and recycle it in a rotary evaporator to recover the acetone solvent. Lignin 11g.
[0040](3) The products of water-insoluble ketone-insoluble lignin and water-insoluble ketone-soluble lignin were vacuum-dried at 40° C. for 20 hours....
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