Olive polyphenol nano-liposome composite membrane and its application in cigarettes
A technology of olive polyphenol nanometer and olive polyphenol resin, which is applied in the fields of application, tobacco, and smoke oil filter elements, etc., to achieve the effects of reducing content, improving sensory score, and good dispersibility
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Embodiment 1
[0029] Preparation of olive polyphenol nanoliposome composite film and composite filter rod.
[0030]1. Take 20 mg of olive polyphenols with a purity of 97.8%, dissolve in 50 mL of 0.05 mol / L phosphate buffer, and prepare an olive polyphenol solution. Accurately draw 20mL of olive polyphenol solution, dissolve 16mg of Tween 80 in it, heat to 60°C and keep constant temperature, stir vigorously to obtain olive polyphenol emulsion. According to the total mass of phospholipid and cholesterol is 24mg, and the mass ratio of phospholipid and cholesterol is 3:7, dissolve in 10mL of 60°C dehydrated ethanol, use a syringe to inject at a constant speed into the olive polyphenol emulsion at a constant temperature, keep the system at a constant temperature, and stir 5min to form an emulsified olive polyphenol liposome suspension. The obtained olive polyphenol liposome suspension was placed in a 500 mL round bottom flask, concentrated under reduced pressure at 0.01 MPa for 30 min, and the ...
Embodiment 2
[0037] Repeat Example 1, with the following differences: the olive polyphenol sample size is 15 mg, the mass ratio of phospholipids to cholesterol is 2:8, and the amount of absolute ethanol is 8 mL.
Embodiment 3
[0039] Repeat Example 1, with the following differences: the olive polyphenol sample size is 15mg, the mass ratio of phospholipid and cholesterol is 4:6, the absolute ethanol consumption is 8mL, the DHMP treatment pressure is 300Mpa, and the olive polyphenol nanoliposome composite membrane Add evenly to the opened cellulose acetate tow at a mass ratio of 15%.
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