Preparation method of palladium-copper alloy film with controllable components and thickness, palladium-copper alloy film and application
A technology of palladium-copper alloy and palladium film, which is applied to the preparation of palladium-copper alloy film with controllable composition and thickness and the field of palladium-copper alloy film and application, can solve problems such as difficulties, achieve accurate control, save production cost, high Effect of Low Temperature Hydrogen Permeability
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[0047] Example 1
[0048] ECN1 porous ceramic material as carrier, 4μm thick Pd 50 Cu 50 Preparation of alloy film
[0049] 1. Preparation of copper plating solution
[0050] Use HFA2004 analytical balance to weigh 30gNa 2 Dissolve EDTA in 400ml of warm water at 40℃-50℃ and record it as solution A for later use. Weigh 10g CuSO 4 ·5H 2 O is dissolved in 100ml of warm water at 40℃, and it is recorded as solution B. Add A to B with slow stirring. In the blue transparent solution, blue precipitation is produced and becomes turbid. The reaction equation is:
[0051] Cu 2+ +2OH - →Cu(OH) 2 ↓Cu 2+ +Na 2 EDTA→CuEDTA+2Na +
[0052] Cu(OH) 2 +Na 2 EDTA→CuEDTA+2NaOH
[0053] Weigh 23g Na 2 CO 3 Dissolve in 100ml of warm water at 40℃. Denote it as solution C. Add C to B slowly by stirring. The blue precipitate previously produced gradually disappears and the solution becomes clear again. Ultrasound for 5 minutes to make the solution mixed more evenly. Weigh 40mg C 10 H 8 O 2 Dissolve in 40ml d...
Example Embodiment
[0070] Example 2
[0071] NJ1 porous ceramic material as carrier, 4μm thick Pd 47 Cu 53 Preparation of alloy film
[0072] 1. Preparation of copper plating solution
[0073] The method is the same as in Example 2.
[0074] 2. Preparation of palladium bath
[0075] The method is the same as in Example 2.
[0076] 3. Carrier pretreatment
[0077] The length of the NJ porous ceramic carrier tube is 67.90mm, the outer diameter is 12.50mm, and the inner diameter is 8.05mm. First in Na 2 CO 3 Soak in the alcohol solution for 30 minutes to remove the oil on the surface. Then soak in deionized water, and vacuum for 15 minutes to remove residual Na 2 CO 3 After treatment, the carrier is white and bright. After that, it is dried in an oven at 150°C for use.
[0078] Activate the dried carrier, immerse it in a reducing agent (dimethylaminoborane), reduce it for 3 to 5 minutes, rinse the carrier tube with distilled water, and then immerse it in a mixture of palladium sulfate and borax to activate t...
Example Embodiment
[0086] Example 3
[0087] ECN2 porous ceramic material as carrier, 5μm thick Pd 45 Cu 55 Preparation of alloy film
[0088] 1. Preparation of copper plating solution
[0089] The method is the same as in Example 2.
[0090] 2. Preparation of palladium bath
[0091] The method is the same as in Example 2.
[0092] 3. Carrier pretreatment
[0093] The ECN porous ceramic carrier tube has a length of 80.25mm, an outer diameter of 14.00mm, and an inner diameter of 11.05mm. First in Na 2 CO 3 Soak in the alcohol solution for 30 minutes to remove the oil on the surface. Then soak in deionized water, and vacuum for 15 minutes to remove residual Na 2 CO 3 After treatment, the carrier is white and bright. After that, it is dried in an oven at 150°C for use.
[0094] Activate the dried carrier, immerse it in a reducing agent (dimethylaminoborane), reduce it for 3 to 5 minutes, rinse the carrier tube with distilled water, and then immerse it in a mixture of palladium sulfate and borax to activate t...
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