Clean production method of titanium dioxide and titanium yellow powder
A technology of titanium dioxide and titanium yellow powder, which is applied in the directions of titanium dioxide, chemical instruments and methods, titanium oxide/hydroxide, etc., can solve the problems of low utilization rate of resources, pollute the environment, a large amount of waste gas and waste water, etc., to reduce the discharge of three wastes and save energy Production cost and energy consumption, the effect of saving production cost
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[0036] The invention provides a method for clean production of titanium dioxide and titanium yellow powder, comprising the following steps:
[0037] a. Mechanical activation of titanium fine powder
[0038] Mill the titanium fine powder for more than 1.5 hours, and make the 400-mesh sieve ≤0.2%, and make activated titanium fine powder;
[0039] b. Normal pressure acid hydrolysis
[0040] Take the activated titanium fine powder prepared in step a, add concentrated hydrochloric acid, heat to 85-95°C, and carry out acidolysis reaction;
[0041] c. Hot filtration and extraction
[0042] Filter the material after acid hydrolysis in step b, wash the filter cake with dilute hydrochloric acid and water for 1 to 3 times, extract the filtrate with a composite extractant, and separate the titanium liquid and iron;
[0043] d. Hydrolysis of titanium liquid
[0044] Heat the titanium solution obtained in step c to 85-95°C, pour it into a hydrolysis pot pre-installed with hot water, and...
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