PVB based 3D printing wire material and preparation method thereof
A 3D printing and wire technology, applied in the field of 3D printing, can solve the problems of inconvenient use and unfavorable product appearance, and achieve the effects of good light transmission, improved surface finish, and simple preparation methods
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Embodiment 1
[0015] It consists of the following raw materials in parts by weight: 100 parts of PVB resin, 3 parts of compatibilizer, 1.5 parts of paraffin oil, 5 parts of antioxidant and 2.5 parts of plasticizer. The molecular weight distribution coefficient of the PVB resin is 2.2, the number average molecular weight is 160,000, the mass fraction of vinyl alcohol groups is 17%, the degree of acetalization is 77%, and the melt index is 5.
[0016] The preparation method of the PVB-based 3D printing wire, the specific steps are as follows:
[0017] Step 1: Weigh the materials, mix them in a high-speed mixer for 10 minutes, control the rotation speed at 240r / min, then dry them in a vacuum oven at 80°C for 8 hours, and set aside;
[0018] Step 2, import the dried raw materials into a single-screw extruder, control the temperature of the extruder at 180°C, and the temperature of the extruder head at 175°C, melt the raw materials, and extrude them through the single-hole extrusion head;
[00...
Embodiment 2
[0021] It consists of the following raw materials in parts by weight: 100 parts of PVB resin, 4 parts of compatibilizer, 2.5 parts of paraffin oil, 6 parts of antioxidant and 4 parts of plasticizer. The compatibilizer is a mixture of EVA and EVA-g-MAH; paraffin oil is a hydrocarbon mixture with 24 carbon atoms; the antioxidant is a compound system of hindered phenolic antioxidant and phosphite antioxidant; The plasticizer is a compound of triethylene glycol di-2-ethylhexanoate, diethylene glycol dibenzoate and triphenyl phosphate.
[0022] The preparation method of the PVB-based 3D printing wire, the specific steps are as follows:
[0023] Step 1: Weigh the materials, mix them in a high-speed mixer for 15 minutes, control the speed at 300r / min, then dry them in a vacuum oven at 80°C for 5-8 hours, and set aside;
[0024] Step 2, import the dried raw materials into a single-screw extruder, control the temperature of the extruder at 160°C, and the temperature of the extruder he...
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