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Humidity sensor film based on microregion redissolution reaction and preparation method thereof

A humidity sensor and redissolving technology, applied in the field of composite materials and humidity sensors, can solve the problems of the process method to reduce the sensor's hysteresis performance, the composite material cannot be fully dispersed, and the hysteresis performance is low, so as to improve the humidity sensitivity performance, fast Effective adjustment and improvement, easy access to materials

Inactive Publication Date: 2017-06-30
UNIV OF ELECTRONICS SCI & TECH OF CHINA
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] However, the above reports have little research on the hysteresis performance, and do not involve the process of how to reduce the hysteresis performance of the sensor.
In the process of material compounding, in order to enhance the hysteresis performance, it is often necessary to have strong interaction forces (such as chemical bonds, ionic bonds, etc.) As a result, insoluble matter is generated and solid phases such as precipitation are formed, so that the composite material cannot be fully dispersed and prepared on the surface of the substrate by the solution method

Method used

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  • Humidity sensor film based on microregion redissolution reaction and preparation method thereof
  • Humidity sensor film based on microregion redissolution reaction and preparation method thereof
  • Humidity sensor film based on microregion redissolution reaction and preparation method thereof

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preparation example Construction

[0040] A method for preparing a humidity sensor thin film based on a micro-region redissolution reaction, comprising the following steps:

[0041] ① Carry out standard cleaning procedures on the substrate used for film formation;

[0042] ② Preparing a thin film of the leading layer on the surface of the cleaned substrate;

[0043] ③Drying the film of the leading layer;

[0044] ④Prepare the backward layer film on the leading layer film: Drop the solution B onto the leading layer film with micron level droplets, the solute in the solution B will react chemically or ionicly with the leading layer film, after the solvent in the solution B volatilizes Finally, the backward layer film is formed.

[0045] When preparing the leading layer film, solution A is added to the gas atomization spray gun or other atomization equipment, and the solution flow is generated inside the spray gun by gas atomization, so that the solution A is transformed from the original flow state into a micro...

Embodiment 1

[0052] This embodiment adopts as figure 1 The standard air-jet method is shown to prepare graphene oxide / polyethyleneimine moisture-sensitive films. Through the air-jet airbrush, the solution A and solution B added to the airbrush spray chamber are brought out by the bearing effect of the nitrogen gas flow, and are atomized in the airbrush nozzle by using the air pressure, spray the airbrush, and in the air flow And under the action of gravity, it is deposited on the surface of the device to complete the preparation of the humidity sensitive film.

[0053] In this case, a quartz crystal microbalance (QCM) device was chosen as the substrate for thin film preparation.

[0054] In this case, the moisture-sensitive materials and concentrations used are: solution A: a polyethyleneimine solution with a concentration of 0.1% (w / v) obtained by adding ultrapure water with a resistance of 15.0MΩ; solution B: a concentration of 0.1mg / ml graphene oxide solution prepared by Hummer method...

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Abstract

The invention discloses a humidity sensor film based on a microregion redissolution reaction and a preparation method thereof, and belongs to the technical field of the composite material and humidity sensor. The preparation method comprises the following steps: based on the technology and feature of an atomization process, such as the gas release, dissociating uniform solution to micron-type microdrops, conveying the microdrops to a film formation substrate by the gas, forming the micron-type redissolution reaction microregion in the guide layer film, and reacting by two or more materials in the microregion and finishing the film deposition process. The preparation method is capable of overcoming the problem in the traditional film preparation process that two or more materials cannot form the film because of the reaction deposition between the materials or the bad effect of the solution dispersion state caused by the generation. The humidity-sensitivity film prepared by the preparation method is capable of obviously improving the sensor feature characters, such as wet hysteretic property, because of the physical and chemical reactions, such as the bonding between the materials, and the electrostatic adsorption.

Description

technical field [0001] The invention relates to the field of composite materials and humidity sensors, in particular to a method for improving hysteresis of a thin-film humidity sensor based on a micro-region redissolution reaction. Background technique [0002] Humidity is one of the important parameters for environmental monitoring. It is difficult to measure humidity accurately, because humidity is an independent parameter, and the water vapor content in the air is very small, and it is difficult to concentrate on the surface of the humidity sensitive element, so it has to be separated according to the laws of physics and chemistry. The humidity value can only be obtained by converting to measuring secondary parameters related to humidity and then converting them. However, these secondary parameters are greatly affected by other factors such as atmospheric pressure and temperature, which makes humidity measurement more difficult. With the gradual deepening of people's un...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N29/02
CPCG01N29/022G01N2291/02845
Inventor 太惠玲袁震叶学亮谢光忠杜晓松蒋亚东
Owner UNIV OF ELECTRONICS SCI & TECH OF CHINA
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