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205results about How to "High film forming efficiency" patented technology

Rare-earth modified Ti-Zr chemical passivation solution for surface treatment of aluminium profiles and using method of rare-earth modified Ti-Zr chemical passivation solution

The invention discloses a rare-earth modified Ti-Zr chemical passivation solution for surface treatment of aluminium profiles and a using method of the rare-earth modified Ti-Zr chemical passivation solution. The rare-earth modified Ti-Zr chemical passivation solution is characterized in that the passivation solution is a main salt for auxiliary film-formation, which takes rare-earth compounds as a Ti-Zr passivation treatment solution, and a passivation film is light yellow in appearance and has field judgement property on the quality of a formed film. A formula of the rare-earth modified Ti-Zr chemical passivation solution is as follows: each litre of solution contains 0.5g.L<-1>-10g.L<-1> of potassium fluotitanate (hexafluorotitanic acid), 0.5g.L<-1>-10g.L<-1> of potassium fluozirconate (fluozirconic acid), 0.5g.L<-1>-5g.L<-1> of cerium nitrate (ceric sulfate and ammonium ceric nitrate), 2g.L<-1>-10g.L<-1> of potassium nitrate, 0.5g.L<-1>-3g.L<-1> of sodium fluoride (potassium fluoride), 0.5g.L<-1>-1g.L<-1> of sodium dodecyl benzene sulfonate or OP-10, 0.2mL-5mL.L<-1> of nitric acid and 1g.L<-1>-5g.L<-1> of boric acid. The using method of the rare-earth modified Ti-Zr chemical passivation solution comprises the following steps of: (1) clearing dirt, such as dirt attached to an aluminium alloy; (2) pretreating the surface of the aluminium alloy; (3) carrying out passivating treatment on the surface of the aluminium alloy by using the rare-earth modified Ti-Zr chemical passivation solution; and (4) washing the aluminium alloy by using water and drying the aluminium alloy. The rare-earth modified Ti-Zr chemical passivation solution disclosed by the invention has the advantages of light yellow appearance, high film formation speed, simple process, uniformity in film layer, strong corrosion resistance, low environment pollution and the like.
Owner:GUANGDONG XINGFA ALUMINUM

Chromium-free treating liquid for preparing erosion-resisting oxide film on aluminum alloy surface, treating and using method thereof

The present invention discloses a chromium-free treatment liquid for preparing corrosion resistant oxidation film at aluminium alloy surface as well as the processing and use method thereof, characterized in that said treatment fluid utilizes a cobalt (III) salt as a main salt and a hypermanganate and a nitrate as a composite oxidizing compound to prepare a composite Co-Mn oxidation film having favorable corrosion resistance performances at aluminium alloy surface. The formula for said treatment liquid is that each litre solution contains cobalt salt of 5 g / L(-1)-20 g / L(-1), kalii permangana of 1 g / L(-1)-4 g / L(-1), sodium nitrate of 1 g / L(-1)-4 g / L(-1), promotor (chlorides and fluorides) of 1 g / L(-1)-4 g / L(-1), sodium acetate of 20 g / L(-1)-50 g / L(-1) and wetting agents (sodium dodecylbenzene sulfonate, OP-10) of 0.5 g / L(-1)-1 g / L(-1). Saic processing and use method comprises (1)sanding the aluminium alloy until its surface is smooth and even; (2) pretreating the aluminium alloy surface; (3) performing a conversion processing by using the treatment fluid; (4) cleaning-up using water and atmospheric-drying naturally. Said treatment fluid in accordance with the present invention possesses the advantages of environmental protection due to its hexavalent chromium-free, fast film-forming speed, simple process, uniform rete, strong corrosion resistance, few environment pollution, and the like.
Owner:GUANGYA ALUMINUM

Environmentally-friendly black chrome-silver-free zinc-plating passivation solution and preparation method thereof

The invention provides black passivation solution for zinc-plating post treatment. 1 liter of black passivation solution consists of 10 to 20g of sodium silicate, 20 to 30g of copper sulfate, 0.5 to 1.5g of nickel sulfate, 0.5 to 1.5g of ferrous sulfate, 1 to 3g of sodium acetate, 20 to 40mL of glacial acetic acid, 3 to 7mL of sulfuric acid (98 percent) and the balance of water. A zinc-plating material processed by the passivation solution has a uniform, bright and black appearance and high corrosion resistance, is free of rust for over 200h through a neutral salt spray test and can achieve the same effect as that achieved by the conventional black chrome-silver-contained passivation process in appearance and performance. The passivation solution has the advantages of thoroughly solving the problem of environment pollution caused by a chromium salt used by the conventional black zinc-plating passivation process, eliminating the use of a silver salt at the same time and greatly reducing the cost thereof by substituting silicate for the chromium salt as a main film-forming material and a copper salt, a nickel salt and a ferric salt for the silver salt as a blackening agent, along with stability and reliability and high film-forming efficiency.
Owner:KUNMING UNIV OF SCI & TECH

Preparation method for directly generating hydroxyapatite-containing biological ceramic membrane on surface of titanium

The invention discloses a preparation method for directly generating a hydroxyapatite-containing biological ceramic membrane on the surface of titanium, and aims to solve the practical problems that the prior art is complex in process, time-consuming, low in electrolyte utilization ratio, poor in membrane forming efficiency and the like. The preparation method adopts a basic method of micro-arc oxidation, and is characterized in that during the preparation of electrolyte, low-solubility calcium dihydrogen phosphate is used for providing phosphate anions and citric acid is used as a complexing agent. Compared with the prior art, although the solubility of the calcium dihydrogen phosphate used in the preparation method is low, the solubility of the calcium dihydrogen phosphate is improved after the calcium dihydrogen phosphate is complexed with the citric acid, calcium ions and phosphate anions are provided at the same time, the utilization ratio of the electrolyte is high, the reaction speed is high, the membrane forming efficiency is high, the preparation method is simple and easy to operate and low in cost, the hydroxyapatite-containing biological ceramic membrane prepared by the preparation method is stable in structure, uniform in distribution and high in effective matter content, and has a wide prospect in the fields of hard tissue implants, tooth planting and the like.
Owner:JILIN UNIV

Tube alignment type condensation polymerization reaction kettle

The invention discloses a tube alignment type condensation polymerization reaction kettle. According to the kettle, tube plates (4) are arranged inside a vertical casing (8); the tube plates (4) are connected with a tube alignment (5); material distributors (6) are arranged on the upper end tube openings of the tube alignment (5); annular gaps (7) are arranged between the upper end tube openings of the tube alignment (5) and the material distributors (6); the top end of the vertical casing (8) is provided with a material inlet (1), and the lower end of the vertical casing (8) is provided witha material outlet (10); the lower part of the side surface of the vertical casing (8) is provided with a heating medium inlet tube (2), the upper part of the side surface of the vertical casing (8) is provided with a heating medium outlet tube (3), and the middle-lower part of the side surface of the vertical casing (8) is provided with a vacuum pumping port (9). According to the present invention, material naturally flows downward by gravity, if the tube alignment is large, the film forming of the inner wall of tube alignment is sufficient, such that the blocking problem can not be generated; the tube alignment type condensation polymerization reaction kettle of the present invention has characteristics of good film forming effect, reliable use, and high work efficiency, and can be used for productions of PET and other high viscosity polymers. In addition, a plurality of the tubes can be aligned in the tube alignment.
Owner:ZHEJIANG UNIFULL IND FIBER

Treating solution for preparing Al-Mo-Mn-Re quaternary composite passivation film on aluminum profile surface and its application method

ActiveCN102732870AImprove compactness and comprehensive performanceEfficient and fast film formation at low temperatureMetallic material coating processesChemistryLanthanum nitrate
The invention discloses a treating solution for preparing a corrosion resistant Al-Mo-Mn-Re quaternary composite passivation film on an aluminum alloy surface and its application method. The passivation solution is characterized by being a passivation treatment solution which is used for preparing a passivation film on an aluminum alloy surface by utilizing a molybdate, a rare earth salt and a permanganate oxidant. Per liter of the treating solution consists of: 8g.L<-1>-25g.L<-1> of sodium molybdate (or ammonium molybdate), 5g.L<-1>-10g.L<-1> of potassium permanganate, 0.5g.L<-1>-3g.L<-1> of sodium fluoride (or potassium fluoride), 0.5g.L<-1>-5g.L<-1> of cerium nitrate (or ceric sulfate, lanthanum nitrate), 1g.L<-1>-5g.L<-1> of acetic acid, 0.5g.L<-1>-1g.L<-1> of sodium dodecyl benzene sulfonate (or OP-10) . The application method includes: (1) removing adhered dust and other dirt from the aluminum alloy; (2) then conducting pretreatment on the aluminum alloy surface; (3) using the treating solution for passivation treatment; and (4) carrying out water washing and drying. The treating solution of the invention has the advantages of fast film formation speed, simple process, uniform film, strong corrosion resistance, and less environmental pollution, etc.
Owner:GUANGDONG XINGFA ALUMINUM JIANGXI

A preparation method for lead-free piezoelectricity thick film

The invention discloses a silk screen printing preparation method of a lead-free piezoelectric thick-film, including: (1) the lead-free piezoelectric ceramic powder is prepared by adopting a solid phase method; (2) an adhesive is dissolved in terpineol according to the weight ratio of 3: 100 to 9: 100 so as to obtain an organic mixture; (3) the lead-free piezoelectric ceramic powder and the organic mixture are mixed according to the weight ratio of 15: 10 to 90: 10, a dispersant and a plasticizer are added for mixing, grinding and ball milling so as to obtain a paste which is ready to be printed; (4) the paste is printed on a substrate by adopting a silk screen printing technology, a thick-film blank with needed thickness is obtained by being placed flat, baking, preburning and repeated operation; (5) the blank is treated with sintering below 1050 to 1300 DEG C, and heat preservation is kept for 15 to 45 minutes. The invention has simple technology, environmental protection, high efficiency of film formation, good reproducibility, dense film formation and excellent electrical performances, the thickness can be controlled arbitrarily between 10 and 100Mum, various printing thick-film patterns can be obtained without a lithography technology; the invention is compatible with the MEMS technology and is applicable to the preparation of piezoelectric micro-motors, micro-fluid pumps, ultrasonic transducers and micro-actuators.
Owner:HUAZHONG UNIV OF SCI & TECH

Alloy high temperature oxidation resisting nanostructure conductive coating prepared with spinel powder reduction method

The invention provides a preparing method of an alloy high temperature oxidation resisting nanostructure conductive coating, i.e. a spinel powder reduction coating method. On one hand, coating powdermaterial with favorable sintering performance is obtained by the regulation and control of the preparing process of coating powder material and effective reductive treatment; on the other hand, a nanometer microstructure film is prepared on the alloy surface by adopting silk screen assisted improved sizing agent coating technology. The film has controllable and even thickness and superior performance, and coating is tightly combined with the alloy; the coating alloy has lower area specific resistance (ASR) and higher long-time running stability under high temperature oxidation environment. Thespinel powder reduction coating method originated by the invention has simple film manufacturing method, low cost and strong repetitiveness, can be applied to coating preparation of alloy with different shapes or sizes, has superiority especially when preparing the large-area alloy coating in practical application, can greatly lower the preparing cost of the alloy coating and has strong applicability.
Owner:SHANGHAI INST OF CERAMIC CHEM & TECH CHINESE ACAD OF SCI

Method for controlling micro-arc oxidation electricity parameters under peak current output mode

The invention provides a method for controlling micro-arc oxidation electricity parameters under a peak current output mode, comprising the following steps of: respectively connecting a pre-treated piece as an anode and stainless steel as a cathode with an output port of a direct-current pulse power supply; immersing in micro-arc oxidation electrolyte; setting initial electricity parameters, wherein pulse peak current density is Ip1, pulse width delta is t1; pulse number is N1 and duration time is t1; undergoing an arc discharge phenomenon on the surface of the pre-treated piece within t1 andsimultaneously, forming a ceramic layer on the surface, and beginning to enter a growth thickening stage; in the event of not shutting off the power supply, under the conditions of ensuring that the average current Ia output is as low as possible and the growth of the ceramic layer can be kept, gradually reducing the value of Ip on the basis of Ip1, and gradually increasing the values of delta t and N on the basis of delta t1 and N1 to rapidly thickening the ceramic layer; and, when the ceramic layer achieves the pre-set thickness, taking out a work-piece; washing; and drying. The method disclosed by the invention has the benefits as follows: the heat loss can be reduced; and the smooth and uniform ceramic layer can be obtained.
Owner:NANJING HAORANG ENVIRONMENT SCI & TECH

Hydrophobic heat insulation and cooling film and preparation method thereof

The invention provides a hydrophobic heat insulation and cooling film and a preparation method thereof. The hydrophobic heat insulation and cooling film is a polymer porous film, the porosity is 30% -90%, the interior of the hydrophobic heat insulation and cooling film is of a spongy structure, the pore diameters of pores are distributed in a bimodal mode, and the width distribution of the poresis 0.2 micrometer - 0.6 micrometer and 1 micrometers - 5 micrometers respectively. The preparation method of the hydrophobic heat insulation and cooling film comprises the following steps of dissolving a polymer into an organic good solvent, adding a non-solvent to prepare a precursor solution, and spraying the precursor solution onto a substrate to obtain the hydrophobic heat insulation and cooling film. The hydrophobic heat insulation and cooling film is a flexible film material with good hydrophobicity, good heat insulation effect and good cooling effect, shows very excellent flexible performance, can be bent and curled at will, can be suitable for the surfaces of base bodies with different shapes, can achieve effective cooling and refrigeration inside the base bodies, and is good in application prospect and high in practicability; the preparation method of the hydrophobic heat insulation and cooling film has the advantages of simplicity, feasibility, low production cost, high filmforming efficiency and the like, is suitable for large-scale preparation and is beneficial to industrial application.
Owner:NAT UNIV OF DEFENSE TECH

Independent-type multi-source confocal ultrasonic atomization pyrolysis spraying reaction chamber

The invention discloses an independent-type multi-source confocal ultrasonic atomization pyrolysis spraying reaction chamber. A sample bearing table is arranged in the reaction chamber, a heating body shell is arranged on the upper portion of the sample bearing table, and heating bodies are arranged in the heating body shell; at least two atomization sources are mutually independent and are arranged in the circumferential direction of the reaction chamber, and a spraying nozzle on the upper portion of each atomization source is connected with a spraying pipe; the upper portions of the spraying pipes both face the axis line of the reaction chamber and both form a spraying angle alpha with the axis line of the reaction chamber; and a nozzle at the upper portion of each spraying pipe is provided with a baffle, and the baffles can block or open the spraying nozzles at the upper ends of the corresponding spraying pipes. By means of the independent-type multi-source confocal ultrasonic atomization pyrolysis spraying reaction chamber, a thin film containing required components can be obtained, and the defect of cross contamination caused by a traditional structure is overcome; and high-temperature reaction tail gas near the sample bearing table is hooded through a tail gas pumping hood, heat reflection can be achieved through a heat reflection hood, and cooling is further achieved through a water-cooling heat shield plate.
Owner:CHONGQING UNIV OF TECH
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