Production method for microwave catalytic pyrolysis of Eupatorium adenophorum
A technology of Eupatorium adenophorum and its production method, which is applied in the field of comprehensive resource utilization, can solve the problems of inability to apply dye wastewater adsorbent, ignore the comprehensive utilization of biomass oil, and reduce the utilization rate of resources, so as to achieve circular economy and product added value High, product cleaning effect
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Embodiment 1
[0028] The microwave catalyzed pyrolysis method for producing Eupatorium adenophorum, its specific steps are as follows:
[0029] (1) First put Eupatorium adenophorum in 0.5mol / LFeSO according to the liquid-solid ratio of 3:1g / ml 4 In the solution, soak for 90 minutes under ultrasonic conditions (ultrasonic power is 150W), then filter and dry to obtain Eupatorium adenophorum after soaking;
[0030] (2) Put the Eupatorium adenophorum obtained in step (1) in a microwave oven under a carbon dioxide atmosphere (the amount of carbon dioxide introduced is 150ml / min), and pyrolyze it at 700°C for 90 minutes to obtain gas products and solid products;
[0031] (3) The gas product obtained in step (2) is rapidly condensed at -2°C, and the condensable part is directly condensed into a liquid-phase high-quality biomass oil, which is further processed to obtain a bio-oil fuel, and the non-condensable part is a gas fuel. After treatment, it can be used instead of fuel; the solid product ob...
Embodiment 2
[0034] The microwave catalyzed pyrolysis method for producing Eupatorium adenophorum, its specific steps are as follows:
[0035] (1) First put Eupatorium adenophorum in 0.3mol / LFeSO according to the liquid-solid ratio of 5:1g / ml 4 In the solution, soak for 30 minutes under ultrasonic conditions (ultrasonic power is 50W), then filter and dry to obtain Eupatorium adenophorum after soaking;
[0036] (2) Put the Eupatorium adenophorum obtained in step (1) in a microwave oven under a carbon dioxide atmosphere (the amount of carbon dioxide introduced is 350ml / min), and pyrolyze it at a temperature of 900°C for 30 minutes to obtain gas products and solid products;
[0037] (3) The gas product obtained in step (2) is rapidly condensed at -2°C, and the condensable part is directly condensed into a liquid-phase high-quality biomass oil, which is further processed to obtain a bio-oil fuel, and the non-condensable part is a gas fuel. After treatment, it can be used instead of fuel; the so...
Embodiment 3
[0040] The microwave catalyzed pyrolysis method for producing Eupatorium adenophorum, its specific steps are as follows:
[0041] (1) First put Eupatorium adenophorum in 0.4mol / LFeSO according to the liquid-solid ratio of 4:1g / ml 4 In the solution, immerse under ultrasonic conditions for 60min (ultrasonic power is 100W), then filter and dry to obtain Eupatorium adenophorum after immersion;
[0042] (2) Put the Eupatorium adenophorum obtained in step (1) in a microwave oven under a carbon dioxide atmosphere (the amount of carbon dioxide introduced is 200ml / min), and pyrolyze it at 800°C for 60 minutes to obtain gas products and solid products;
[0043] (3) The gas product obtained in step (2) is rapidly condensed at -2°C, and the condensable part is directly condensed into a liquid-phase high-quality biomass oil, which is further processed to obtain a bio-oil fuel, and the non-condensable part is a gas fuel. After treatment, it can be used instead of fuel; the solid product ob...
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