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Preparation method of cottonseed meal protein compound slurry

A cottonseed meal and protein technology, used in textiles, papermaking, fiber processing, etc., can solve the problems of poor film-forming properties and drying denaturation of protein pulp, limiting the successful application of protein pulp, and achieve good biodegradability. , avoid protein denaturation, increase abrasion resistance and weaveability

Active Publication Date: 2017-07-25
JIANGNAN UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The addition of the two reagents essentially cannot improve the two disadvantages of poor film-forming properties and drying denaturation of the protein size, thus limiting the successful application of the protein size in the sizing process
In addition, in this patent, compounding protein slurry with PVA, especially when the PVA content exceeds 50%, can effectively improve film formation and protein denaturation during drying, but it still cannot completely replace PVA

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024]Completely dehulled cottonseed meal was used as raw material, and the cottonseed meal was detoxified by gossypol with a mass fraction of 10% sodium hydroxide solution. The mass fraction of the cottonseed meal was 50%, the temperature was 60°C, and the treatment time was 1 hour. The detoxified cottonseed meal and corn oxidized starch were mechanically activated in the mechanical activation equipment for 1 hour according to the dry basis mass ratio of 20:1. Then the activated mixture was placed in a reaction system of 3% sodium hydroxide solution and treated with 400 watts of ultrasonic waves for 30 minutes, and the mass fraction of cottonseed meal protein in the reaction system was 10%. The reaction system after ultrasonic treatment was stirred at 85° C. for 10 minutes, and then glycerin, a hydrophilic plasticizer accounting for 20% by mass of cottonseed meal protein, was added. Stirring was continued for 50 minutes at 85°C. Under the condition of keeping warm at 85°C, t...

Embodiment 2

[0031] Using completely dehulled cottonseed meal as raw material, the cottonseed meal was detoxified by gossypol with a mass fraction of 15% sodium hydroxide solution, the mass fraction of cottonseed meal was 75%, the temperature was 80°C, and the treatment time was 2 hours.

[0032] The detoxified cottonseed meal and corn oxidized starch were mechanically activated in the mechanical activation equipment for 1 hour according to the dry basis mass ratio of 15:1, and then the activated mixture was placed in a 4% sodium hydroxide solution reaction system for use 1000 watts of ultrasonic treatment for 10 minutes, the mass fraction of cottonseed meal protein in the reaction system was 20%. The reaction system after ultrasonic treatment was stirred at 90° C. for 30 minutes, and then 30% of the protein mass percentage of cottonseed meal was added to the hydrophilic plasticizer glycerin. Stirring was continued for 60 minutes at 90°C. Under the condition of keeping warm at 90°C, the p...

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PUM

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Abstract

The invention discloses a preparation method of cottonseed meal protein compound slurry. The preparation method comprises the following steps: mixing cottonseed meal, which is treated by detoxification by using gossypol, with starch according to a dry basis mass ratio of (20 to 1) to (10 to 1) to obtain mixed dry powder; putting the mixed dry powder into an alkaline solution, wherein the mass of the alkaline solution is 5-20 times that of the mixed dry powder, and the hydroxyl ion concentration of the alkaline solution is 1-5%; carrying out ultrasonic treatment on the obtained mixture for 5-60min; then, stirring and heating for 30-90min at the constant temperature of 50-95 DEG C, adding a hydrophilic plasticizer in the process of stirring and heating, wherein the mass of the hydrophilic plasticizer accounts for 10-30% of that of the mixed dry powder, using diluted hydrochloric acid to adjust the pH value of a reaction system to a neutral or weak alkaline condition, and removing precipitate to obtain the slurry which is the cottonseed meal protein compound liquid slurry directly used for sizing. After the technical scheme is adopted, the completely unshelled cottonseed meal is prepared into the slurry for warp sizing so as to replace polyvinyl alcohol (PVA), so that the problem that the biodegradation of desizing wastewater is difficult to implement is effectively solved, and the bottleneck that the desizing wastewater is difficult to treat is broken through.

Description

technical field [0001] The invention belongs to the field of sizing materials for warp yarn sizing, and in particular relates to a method for preparing cottonseed meal protein compound sizing materials used for sizing. Background technique [0002] Sizing is an important process in the processing of spun yarn woven fabrics. Dip-type sizing machines are generally used in textile enterprises to sizing yarns. In the sizing process, firstly, the size and additives are compounded according to a certain ratio, and then the sizing and heat preservation gelatinization are carried out at 80-100°C for 30-90 minutes, and then the yarn is liquidized at 80-100°C Dip sizing of size allows the size to enter the interior of the yarn. After the yarn is dipped and sized, it enters a drying room at 100°C-120°C and is dried on a roller, so that the size film forms a size film on the surface of the yarn, which enhances the strength and wear resistance of the yarn and fits the hairiness. , redu...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M15/15D06M13/342D06M15/11D06M13/148
Inventor 刘建立储志超高卫东王鸿博朱博
Owner JIANGNAN UNIV
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