Preparation method of particle self-assembled TiO2/Fe2O3 chain-like compound powder
A composite powder, self-assembly technology, applied in chemical instruments and methods, metal/metal oxide/metal hydroxide catalysts, chemical/physical processes, etc. control effect
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Embodiment 1
[0019] Embodiment 1: Particle self-assembly Fe with a particle diameter of 50nm 2 o 3 Chain powder.
[0020] (1) First, wash the instrument to be used with ethanol and water, then use a 50mL small beaker to weigh 4mmoL ferrocene and 10mmoL glycine with an electronic balance, weigh 10mL ethanol with a graduated cylinder, and add 5mL water into the small beaker , to form solution A; after stirring for about 1 h on a magnetic stirrer, solution B was formed.
[0021] (2) Transfer the stirred mixture into a 25mL reaction kettle that has been washed in advance; cover the reaction kettle and put it in a constant temperature blast drying oven, set the temperature at 180°C, and react for 36 hours; after the reaction is completed, take out the reaction kettle , the powder generated after the reaction was centrifuged with a centrifuge, washed alternately with absolute ethanol and deionized water several times, and then dried at 60 ° C for 6 h to obtain a yellow Fe 2 o 3 powder.
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Embodiment 2
[0023] Embodiment 2: Particle self-assembly Fe with a particle diameter of 200nm 2 o 3 Chain powder.
[0024] (1) First, wash the instrument to be used with ethanol and water, then use a 50mL small beaker to weigh 4mmoL ferrocene and 10mmoL glycine with an electronic balance, weigh 12mL ethanol with a graduated cylinder, and add 3mL water into the small beaker , to form solution A; after stirring for about 1 h on a magnetic stirrer, solution B was formed.
[0025] (2) Transfer the stirred mixture into a 25mL reaction kettle that has been washed in advance; cover the reaction kettle and put it in a constant temperature blast drying oven, set the temperature at 180°C, and react for 36 hours; after the reaction is completed, take out the reaction kettle , the powder generated after the reaction was centrifuged with a centrifuge, washed alternately with absolute ethanol and deionized water several times, and then dried at 60 ° C for 6 h to obtain a yellow Fe 2 o 3 powder.
[...
Embodiment 3
[0027] Embodiment 3: particle diameter is the particle self-assembly Fe of 50nm 2 o 3 / TiO 2 Composite chain powder
[0028] (1) First, wash the instrument to be used with ethanol and water, weigh 0.224g of tetrabutyl titanate (be careful not to encounter water) with an electronic balance, put it into a 50mL small beaker, and then weigh it with a measuring cylinder. Pour 10mL of ethanol into a small beaker and put it into an ultrasonic cleaner for 5 minutes to form solution A; then weigh 4mmol of ferrocene, 10mmol of glycine, and 5mL of water to form solution B; finally put solution B on a magnetic The stirrer was stirred for about 1 h to form solution C.
[0029] (2) Transfer the ultrasonic mixture into a pre-washed 25mL reaction kettle, cover the reaction kettle and put it in a constant temperature blast drying oven, set the temperature at 180°C, and react for 36 hours; after the reaction is completed, take out the reaction kettle , The powder generated after the reactio...
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