Coating for protecting glass and preparation method thereof
A technology for protecting glass and coatings, applied in the coating and other directions, can solve the problems of small adhesion, easy to fall off, low bonding strength, etc., to achieve the effect of enhancing adhesion, non-toxic to human body and environment, and improving smoothness
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Embodiment 1
[0022] Prepare siloxane-modified polyurethane emulsion for use: add 18g of isophorone diisocyanate, 12g of polypropylene glycol, 10g of polytetrahydrofuran ether glycol, 3g of dimethylol butyric acid and 2g of 1,4-butanediol into the flask Mix, then add an appropriate amount of methyl ethyl ketone to the flask to adjust the viscosity, then add 0.1g of dibutyltin dilaurate as a catalyst, stir and react at 80-85°C for 2 hours to prepare a polyurethane prepolymer, add isobutyltriethoxysilane Modify the polyurethane prepolymer, stir for 1-2 hours, cool down to 35-40°C, add triethylamine to neutralize, slowly add the modified prepolymer to deionized water, add diethylenetriamine, and stir , to obtain silicone modified polyurethane emulsion.
[0023] Get 10 parts by mass of deionized water, 0.1 parts by mass of leveling agent, 0.2 parts by mass of dispersant, 0.2 parts by mass of sodium dodecyl naphthalene sulfonate, 0.2 parts by mass of alcohol ester twelve film-forming aids In th...
Embodiment 2
[0025] Get 20 parts by mass of deionized water, 0.15 parts by mass of leveling agent, 0.25 parts by mass of dispersant, 0.3 parts by mass of sodium heptadecyl naphthalene sulfonate, 0.3 parts by mass of alcohol ester twelve film-forming aids In the dispersion kettle, stir at a high speed; add 1.2 mass parts of dipropylene glycol monomethyl ether, 0.14 mass parts of ethyl (methyl) triethoxy (methoxy) silane to the dispersion kettle, stir; Add 0.1 parts by mass of nano-zinc oxide, 0.1 parts by mass of nano-alumina, 0.04 parts by mass of nano-silicon carbide, and 3 parts by mass of reflective powder, stir; then add 35 parts by mass of the prepared in Example 1 to the dispersion kettle The siloxane-modified polyurethane emulsion and 8 parts by mass of acrylic emulsion were stirred, ground and dispersed, and filtered to obtain a coating for protection and retention. The coating film has good water resistance, scrub resistance, scratch resistance, and strong adhesion on the glass su...
Embodiment 3
[0027] Take 20 parts by mass of deionized water, 0.3 parts by mass of leveling agent, 0.3 parts by mass of dispersant, 0.6 parts by mass of dodecylphenol, and 0.5 parts by mass of alcohol ester twelve film-forming aids into the dispersion tank , high-speed stirring; add 2 mass parts of dipropylene glycol monomethyl ether, 0.2 mass parts of ethyl (methyl) triethoxy (methoxy) silane to the dispersion tank, stir; then add 0.1 mass 45 parts by mass of nano-alumina, 0.1 parts by mass of nano-silicon carbide, 3 parts by mass of reflective powder, and 0.1 parts by mass of dyestuff, stir; then add 45 parts by mass of the above-prepared siloxane-modified polyurethane to the dispersion kettle Emulsion, 10 parts by mass of acrylic emulsion, stirring, grinding, dispersing, and filtering to obtain a coating for protection and retention. The coating film has good water resistance, scrub resistance, scratch resistance, and strong adhesion on the glass surface. By adding reflective powder to...
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