A kind of antistatic viscose fiber non-woven fabric and preparation method thereof
A viscose fiber and antistatic technology, applied in the field of non-woven fabrics and its preparation, can solve the problems of poor antistatic performance, low liquid absorption, low cleanliness, etc., achieve good washing resistance, improve antistatic performance, The effect of improving cleanliness
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[0046] 1. The embodiment of preparing epoxy-terminated polyether
[0047] Embodiment 1~4, comparative example 1-1, comparative example 1-2, comparative example 1-3 and comparative example 1-4, prepare epoxy-terminated polyether and common polyether by the prescription of table 1, P1 to P8 were obtained respectively.
[0048] (1) Ring-opening reaction: Add polyether polyol and boron trifluoride ether complex into a 20L glass reactor respectively, and add them within 0.5h at a temperature of 55°C and a stirring speed of 200r / min. Epichlorohydrin, after the addition of epichlorohydrin, keep the heating temperature and stirring speed constant, and react for 2 hours;
[0049] (2) Ring-closing reaction: Cool the above reaction solution to 35°C, add a 40% aqueous sodium hydroxide solution, age for 2 hours, and let stand to separate;
[0050] (3) Purification: take the upper organic layer, evaporate in vacuo to remove unreacted epichlorohydrin, and then carry out vacuum filtration t...
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