Method for preparing biodegradable composite material with high steam barrier property
A technology of water vapor barrier and biodegradation, which is applied in the field of composite materials, can solve the problems of poor barrier performance and failure of barrier performance, and achieve the effect of improving hydrophobicity, reducing swelling and improving water vapor barrier performance
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Embodiment 1
[0033] The raw material of a polycaprolactone (matrix) / glyceryl tristearate (dispersed phase) high water vapor barrier biodegradable composite material comprises the following components and contents by weight:
[0034] Component Parts by weight
[0035] Polycaprolactone (for biodegradable polymer matrix) 80
[0036] Glyceryl tristearate (as the dispersed phase of hydrophobic biodegradable esters) 20
[0037] The first step is to prepare materials according to the above-mentioned components;
[0038] In the second step, the above materials were placed in a vacuum oven at 40 °C for drying for 6 hours;
[0039] In the third step, the dry polycaprolactone and glyceryl tristearate obtained in the second step are placed in a high mixer for premixing for 5 minutes, and the rotating speed is 100 rev / min to obtain polycaprolactone and tristearate. A premix of fatty acid glycerides, the premix was dried in a vacuum oven at 40°C for 3 hours.
[0040] In the fourth step, the polycapr...
Embodiment 2
[0047] The raw material of a polycaprolactone (matrix) / glyceryl tristearate (dispersed phase) high water vapor barrier biodegradable composite material comprises the following components and contents by weight:
[0048] Component Parts by weight
[0049] Polycaprolactone (for biodegradable polymer matrix) 70
[0050] Glyceryl tristearate (as the dispersed phase of hydrophobic biodegradable ester compounds) 30
[0051] The first step is to prepare materials according to the above-mentioned components;
[0052] In the second step, the above materials were placed in a vacuum oven at 40 °C for drying for 6 hours;
[0053] In the third step, the dry polycaprolactone and glyceryl tristearate obtained in the second step are placed in a high mixer for premixing for 5 minutes, and the rotating speed is 100 rev / min to obtain polycaprolactone and tristearate. A premix of fatty acid glycerides, the premix was dried in a vacuum oven at 40°C for 3 hours.
[0054] In the fourth step, the...
Embodiment 3
[0061] The raw material of a polylactic acid (matrix) / glyceryl tristearate (dispersed phase) high water vapor barrier biodegradable composite material comprises the following components and contents by weight:
[0062] Component Parts by weight
[0063] Polylactic acid (for biodegradable polymer matrix) 92
[0064] Glyceryl tristearate (as the dispersed phase of hydrophobic biodegradable esters) 8
[0065] The first step is to prepare materials according to the above-mentioned components;
[0066] In the second step, polylactic acid was placed in a vacuum oven at 80 °C for 6 hours, and glyceryl tristearate was placed in a vacuum oven at 40 °C for 6 hours;
[0067] The 3rd step, the dry polylactic acid and glyceryl tristearate obtained in the second step are placed together in a high mixer for premixing for 5 minutes, and its rotating speed is 100 rev / min to obtain polylactic acid and glyceryl tristearate. The premix was dried in a vacuum oven at 40 °C for 3 hours.
[0068]...
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