Thermal-method powdery electrode printing material and preparation method of printing electrode of thermal-method powdery electrode printing material
A printing material and electrode technology, which is applied to the preparation of thermal powder electrode printing material printing electrodes, and the field of thermal powder electrode printing materials, can solve the problems of difficult electrode shape and scale, slow production speed, and high equipment requirements, and achieves a guaranteed Electrochemical performance, saving of raw materials, simple effect of preparation process
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Embodiment 1
[0036] The graphite, nano-silver wire, phenolic resin, urotropine, and calcium stearate were weighed respectively according to a mass ratio of 94.6:4:1:0.1:0.3. In order to refine the conductive particles and make them uniformly dispersed, the weighed graphite and nano-silver wires were uniformly mixed in a high-efficiency intermittent stirring mixer for 5 minutes to obtain mixed powder A; in order to melt the phenolic resin, coat the conductive On the particle surface, heat the mixed powder A to 90°C under the protection of a nitrogen atmosphere, and then add phenolic resin powder to obtain a mixture B; pass the compressed air into the mixing mixer and stir the mixture B for 10 minutes to refine the powder and make it The phenolic resin is uniformly coated on the surface of the conductive phase powder; the temperature is lowered by 15°C, the aqueous curing agent is added, and stirred for 5 minutes to obtain a mixture C; the temperature is lowered by 15°C again, the lubricant i...
Embodiment 2
[0038] Lithium cobaltate, onion carbon, phenolic resin, urotropine and calcium stearate were weighed in a mass ratio of 92.6:2.5:4:0.4:0.5. In order to refine the conductive particles and make them uniformly dispersed, the weighed graphite and nano-silver wires were uniformly mixed in a high-efficiency intermittent stirring mixer for 30 minutes to obtain mixed powder A; in order to melt the phenolic resin, coat the conductive On the particle surface, heat the mixed powder A to 180°C under the protection of a nitrogen atmosphere, and then add phenolic resin powder to obtain a mixture B; pass the compressed air into the stirring mixer and stir the mixture B for 35 minutes to refine the powder and make it The phenolic resin is evenly coated on the surface of the conductive phase powder; the temperature is lowered to 55°C, the aqueous curing agent is added, and stirred for 15 minutes to obtain the mixture C; the temperature is lowered to 35°C again, the lubricant is added, stirred ...
Embodiment 3
[0040]Weigh lithium cobaltate, onion carbon, phenolic resin, urotropine and calcium stearate at a mass ratio of 89:5:5:0.5:0.5. In order to refine the conductive particles and make them uniformly dispersed, the weighed lithium cobaltate and onion carbon were uniformly mixed in a batch stirring mixer for 20 minutes to obtain mixed powder A; in order to melt the phenolic resin, coat the surface of the conductive particles , heated the mixed powder A to 120°C under the protection of nitrogen atmosphere, then added the phenolic resin powder to obtain the mixture B; passed the compressed air into the mixing mixer and stirred the mixture B for 15 minutes, refined the powder and made the phenolic resin Uniformly coat the surface of the conductive phase powder; lower the temperature by 25°C, add a curing agent aqueous solution, and stir for 5 minutes to obtain a mixture C; lower the temperature again by 25°C, add a lubricant, stir for 5 minutes, and cool to room temperature to obtain t...
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