Circulating fluidized bed system and method for production of hydrogen fluoride from fluorite powder
A circulating fluidized bed and fluorite powder technology, which is applied in the field of circulating fluidized bed technology, can solve the problems of excessive dispersant entrainment and difficulty in separation, and achieve the goal of inhibiting particle agglomeration and wall sticking, low conversion rate and high degree of wear Effect
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Embodiment 1
[0035] The mixed gas of sulfur trioxide, water vapor and HF with a molar ratio of 1:1:1.5 is used as the raw material gas, preheated to 300 degrees Celsius, at 10.0m 3 / h gas velocity enters the reactor inlet pipe, mixes with circulating solids and enters the reactor for reaction. The reactor operates at a temperature of 350 degrees Celsius and a pressure of 1.2 bar. The output reaction product with incompletely reacted solid enters the circulation part, and enters a cyclone separator to separate incompletely reacted solid particles with larger particle size. The pressure drop of the primary cyclone separator is 0.05bar. Sinking solids enter the solids settling section, while gases and smaller solid particles with high conversion rates enter the solids separation section. The solid entering the solid settling section enters the inlet pipe through the lower inclined pipe and the control valve on it, mixes with the reaction gas and circulates back to the reactor. The length o...
Embodiment 2
[0039] Sulfuric acid vapor with a mass fraction of 98% and HF gas are mixed at a molar ratio of 1:1.5 as raw material gas, preheated to 350 degrees Celsius, and 8.0m 3 / h gas velocity enters the reactor inlet pipe, mixes with circulating solids and enters the reactor for reaction. The reactor operates at a temperature of 350 degrees Celsius and a pressure of 0.95 bar. Micro-negative pressure can reduce the chance of leakage of dangerous reactants and products. The reaction product with incompletely reacted solids produced by the reactor enters the circulation part, and the incompletely reacted solid particles with larger particle sizes are separated by the primary cyclone separator. The pressure drop of the primary cyclone separator is 0.05 bar. Sinking solids enter the solids settling section, while gases and smaller solid particles with high conversion rates enter the solids separation section. The solid entering the solid settling section enters the inlet pipe through th...
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