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A spinosad fermentation method for improving cell activity

A spinosyn and fermentation method technology, which is applied in the field of biological pesticide preparation, can solve the problems of unsatisfactory spinosyn fermentation yield and other problems, and achieve the effects of obvious economic benefit and value, increase fermentation yield, and improve cell activity.

Active Publication Date: 2021-01-05
QILU PHARMA INNER MONGOLIA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Based on the yield of spinosyn fermentation is not ideal in China, it is a great challenge for the realization of industrialization and industrialization. It is urgent to provide an effective method to increase the yield of spinosad fermentation

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] A spinosad fermentation method for improving cell activity, comprising steps as follows:

[0029] (1) After the experimental verification of the strains producing spinosad, the glycerin tube passed through the seed bottle and fermented for 2-3 days. Microscopic examination showed no bacteria. The shape of the bacteria was radial without breaks. It is 6.8, grow to maturity, obtain seed liquid; carry out next step fermentation.

[0030] (2) Add seed medium into a 30-liter seed tank, cool to 30°C after sterilization, and carry out aseptic pressure holding, and then under the protection of the flame, put the seed liquid into the seed tank for seed cultivation, the inoculation amount 50ml, the seed tank culture conditions are: temperature 30°C, tank pressure 0.05Mp, ventilation rate 1vvm, pH between 7-8, culture for 2-3 days, stirring speed 300 rpm, dissolved oxygen general seed tank maintenance Above 80%, the raw material formula of the seed medium is composed as follows i...

Embodiment 2

[0035] A spinosad fermentation method for improving cell activity, comprising steps as follows:

[0036] (1) After the experimental verification of the strains producing spinosad, the glycerol tube passed through the seed bottle and fermented for 2-3 days. Microscopic examination showed no bacteria, the shape of the bacteria was radial, no breaks, the bacterial concentration reached more than 20%, and the pH It is 6.8, grow to maturity, obtain seed liquid; carry out next step fermentation.

[0037] (2) Add seed culture medium into a 3000-liter seed tank, cool to 30°C after sterilization, and carry out aseptic pressure holding, and then under the protection of flame, put the seed liquid into the seed tank for seed cultivation, the inoculation amount The seed tank culture conditions are: temperature 30°C, tank pressure 0.05Mp, ventilation volume 1vvm, pH between 7-8, culture for 2-3 days, the stirring speed is 100 rpm for the first 0-10 hours, and then the stirring speed For 25...

experiment example

[0043] Ten batches of fermenters were selected, and zinc sulfate and cobalt chloride were added to the basic material, and the cell activity and potency of spinosad were measured at various time periods during the fermentation of spinosyn fermenters.

[0044] Cell viability assay method: MTT staining method was used to measure absorbance with a microplate reader to measure cell viability.

[0045] Potency test method: high performance liquid chromatography, according to the method specified in the national standard GB29696-2017.

[0046] In summary, the addition of metal trace elements zinc sulfate and cobalt chloride to spinosyn fermentation can significantly improve cell activity, and also significantly increase the yield of spinosad. Plays an important role in fermentation production.

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Abstract

The invention relates to a spinosad fermentation method for improving cell activity. The method comprises: adding zinc sulfate and cobalt chloride to the fermentation medium before the fermentation medium is sterilized, mixing them evenly with the fermentation medium, fully dissolving them, and then Disinfection and sterilization are carried out; after the sterilization, the seed liquid is grown in shake flasks, and after maturation, it is inserted into a seed tank, fermented and matured by the seed tank and then transferred to a fermenter, and the fermentation adopts secondary fermentation. The present invention makes full use of the metal trace elements of zinc sulfate and cobalt chloride to greatly improve the enzymatic activity of killing cells, and through the influence of zinc ions and cobalt ions on the enzyme activity of Saccharopolyspora spinosa cells, thereby affecting Its cell activity makes the cell activity of the multikiller significantly improved, and finally the fermentation titer is greatly improved.

Description

technical field [0001] The invention relates to a spinosyn fermentation method for improving cell activity, and belongs to the technical field of biological pesticide preparation. Background technique [0002] Spinosad is produced by the fermentation of Saccharopolyspora spinosa. Spinosyn is a new type of green broad-spectrum biopesticide, which belongs to microbial source biochemical pesticides. Spinosad has both the safety of biological pesticides and the quick effect of chemically synthesized pesticides. It works on the same day after spraying. The safe harvest period registered by the Ministry of Agriculture in China and the United States is only one day, which is most suitable for the production of pollution-free vegetables. Spinosyn won the US Presidential Green Chemical Challenge Award for its low toxicity, low residue, harmlessness to natural enemies of pests, and fast natural decomposition speed. Today, with increasing awareness of environmental protection and saf...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C12P19/62C12R1/01
CPCC12P19/62
Inventor 连剑飞居亚东翟晓云樊乐李学洋
Owner QILU PHARMA INNER MONGOLIA