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Preparation method of phosphatized anti-corrosive corrugated pipe

A technology of bellows and uniform mixing, which is applied in the field of bellows, can solve the problems of poor compatibility between flame retardants and resins, and reduce the stability and strength of finished bellows, so as to improve compatibility, improve mechanical properties, and good surface activity Effect

Inactive Publication Date: 2017-12-01
马荧莹
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] Application number 201510230205.3 discloses a single-wall corrugated pipe manufacturing process, including the following steps: S1, the following parts by weight of hot melt adhesive 50-70, polyolefin resin 30-50, tackifying resin 3-5, compound Stabilizer 1.2-2, flame retardant 1-2, reinforcing agent 5-30, compatibilizer 0.02-0.05, toughening agent 5-8, add in the internal mixer of airtight high-speed operation; S2, in step S1 After the mixture is kneaded and granulated at 100-140°C with an internal mixer, it is put into a single-screw extruder, extruded at 100-150°C, pelletized, and air-cooled; S3, the obtained in step S2 The pellets and the hot melt adhesive are melted separately and then co-extruded into a double-wall casing. In this method, the compatibility between each flame retardant and the resin is poor, and it is easy to reduce the stability and strength of the finished corrugated pipe.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A preparation method for phosphating anticorrosion bellows, comprising the following steps:

[0022] (1) Take 2 parts by weight of 2-methyl-4-isothiazolin-3-one, add it to deionized water 30 times its weight, stir evenly, add 4 parts by weight of stearic acid, Keep warm for 2 hours, add 2 parts by weight of sodium diacetate, keep warm and stir for 20-30 minutes to obtain carboxylated anticorrosion solution;

[0023] (2) Take 14 parts by weight of montmorillonite, calcinate at 760°C for 2 hours, cool to room temperature, mix with 3 parts by weight of calcium propionate, add to deionized water 7 times the weight of the mixture, stir evenly, drop Add ammonia water with a concentration of 11%, raise the temperature to 65°C after the dropwise addition, and keep stirring for 40 minutes to obtain a hydroxy-montmorillonite solution;

[0024] (3) Get 2 parts by weight of benzotriazole, add it to 6 times the weight of absolute ethanol, stir evenly, add 4 parts by weight of allyl...

Embodiment 2

[0029] (1) Take 1 weight part of 2-methyl-4-isothiazolin-3-one, add it to 24 times its weight in deionized water, stir evenly, add 2.8 weight parts of stearic acid, at 70 ° C Insulate for 1 hour, add 0.7 parts by weight of sodium diacetate, insulate and stir for 20 minutes to obtain a carboxylated antiseptic solution;

[0030] (2) Take 10 parts by weight of montmorillonite, calcinate at 700°C for 1 hour, cool to room temperature, mix with 2 parts by weight of calcium propionate, add to deionized water 5 times the weight of the mixture, stir evenly, drop Add ammonia water with a concentration of 10%, raise the temperature to 60° C. after the dropwise addition, and keep stirring for 30 minutes to obtain a hydroxy-montmorillonite solution;

[0031] (3) Get 1 weight portion of benzotriazole, add it to 4 times its weight in dehydrated alcohol, stir evenly, add 2 weight portions of allyl polyethylene glycol, and keep stirring at 50°C for 10 minutes , to obtain a complex alcohol dis...

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PUM

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Abstract

The invention discloses a preparation method of a phosphatized anti-corrosive corrugated pipe. According to the preparation method of the phosphatized anti-corrosive corrugated pipe, phosphatized anti-corrosive montmorillonoid achieves the antibacterial properties of 2-methyl-4-isothiazolin-3-ketone, sodium diacetate and benzotriazole, the fire-retarding property of tetrakis hydroxymethyl phosphonium sulfate as well as the high-strength characters of montmorillonoid, and meanwhile, obtains excellent surface activity and can effectively improve compatibility with polymer matrix and the anti-bacteria, fire-retarding and mechanical properties of finish pipe products.

Description

technical field [0001] The invention belongs to the field of corrugated pipes, and in particular relates to a preparation method of phosphating anticorrosion corrugated pipes. Background technique [0002] Polymer materials are mainly composed of carbon, hydrogen and other elements. Most of the polymer materials themselves are not flame retardant. great harm; [0003] Polyethylene corrugated pipe is a new type of pipe with a special shaped cross-section ring corrugated structure, which can replace ordinary plastic pipes and other material pipes, and can be used as building wire casings, farmland water conservancy seepage drainage pipes, cable guide pipes, casings, etc.; [0004] Polyethylene is a typical polymer material. Like most polymer materials, it is flammable. The limiting oxygen index of common polyethylene materials is between 18-20%. For the safety of fire prevention, polymer materials usually have a limit oxygen index of at least above, and some special occasion...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/06C08K13/06C08K9/04C08K3/34C08K5/47C08K5/098C08K5/3475
CPCC08K13/06C08K3/346C08K5/098C08K5/3475C08K5/47C08K9/04C08L2201/02C08L2203/18C08L2207/062C08L23/06
Inventor 马荧莹
Owner 马荧莹
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