Deoxidizing agent for steelmaking and preparation method thereof
A technology of deoxidizer and calcium oxide, which is applied in the field of steelmaking additive preparation, can solve the problem of low deoxidation efficiency and achieve the effect of reducing oxygen content
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example 1
[0025] Put the straw into the pulverizer for 30 minutes to obtain rice straw powder, take 1kg of rice straw powder and add it to the retort, raise the temperature to 260°C at a heating rate of 10°C / min, keep the heat for 60min, and wait for the material in the retort to cool down to At room temperature, the dry distillation product was obtained, and the dry distillation product, 10g polyvinyl alcohol and 400mL water were added to the beaker, stirred and mixed for 3 minutes to obtain a mixed solution, the mixed solution was placed in a mold, and pressed for 5 minutes under a pressure of 30MPa to obtain a masterbatch. The masterbatch is placed in a carbonization furnace, and hydrogen gas is introduced into the carbonization furnace, and the rate of hydrogen gas introduction is controlled at 5mL / min. Under the hydrogen protection state, the carbonization is carried out at 400°C for 1 hour, and then naturally cooled to room temperature, and the introduction of hydrogen gas is stoppe...
example 2
[0027]Put the straw into the pulverizer and pulverize it for 35 minutes to get straw powder. Take 2kg of straw powder and add it to the retort, raise the temperature to 270°C at a heating rate of 13°C / min, keep it warm for 75min, and wait for the material in the retort to cool down with the furnace. to room temperature to obtain a dry distillation product, put the dry distillation product, 13g sodium dodecylsulfonate and 450mL water into a beaker, stir and mix for 4min to obtain a mixed solution, put the mixed solution in a mold, and press it under a pressure of 35MPa for 8min , to obtain the masterbatch, put the masterbatch in a carbonization furnace, and pass ammonia gas into the carbonization furnace, control the rate of ammonia gas introduction to 8mL / min, and keep carbonization at 430°C for 2h under the protection of ammonia gas, and then Naturally cool to room temperature, stop feeding ammonia gas to obtain carbonized material, put the carbonized material in a pulverizer ...
example 3
[0029] Put the straw into the pulverizer and pulverize it for 40 minutes to get straw powder. Take 2kg of straw powder and add it to the retort, raise the temperature to 280°C at a heating rate of 15°C / min, keep it warm for 90 minutes, and wait for the material in the retort to cool with the furnace. to room temperature to obtain a dry distillation product, put the dry distillation product, 7g polyvinyl alcohol, 8g sodium dodecylsulfonate and 500mL water into a beaker, stir and mix for 5min to obtain a mixed solution, put the mixed solution in a mold, The masterbatch was pressed under the pressure of 10min to obtain the masterbatch, and the masterbatch was placed in the carbonization furnace, and ammonia gas was introduced into the carbonization furnace, and the rate of ammonia gas introduction was controlled at 10mL / min. Insulate and carbonize for 2 hours, then cool naturally to room temperature, stop feeding ammonia gas to obtain carbonized material, put the carbonized materi...
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